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Smokeless sulfur-free display shell lift-off agent and preparation method thereof

A technology of fireworks bombs and medicaments, which is applied in the field of civil entertainment pyrotechnics, can solve the problems of poor safety and pollution of medicaments, and achieve the effects of low cost, no pollution in the production process, and mature and stable preparation process

Pending Publication Date: 2020-04-03
江西吉润花炮新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a smokeless and sulfur-free fireworks bomb lift-off agent and its preparation method in order to solve the problems of poor safety and serious pollution in the current fireworks bomb lift-off agent

Method used

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  • Smokeless sulfur-free display shell lift-off agent and preparation method thereof
  • Smokeless sulfur-free display shell lift-off agent and preparation method thereof
  • Smokeless sulfur-free display shell lift-off agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A smokeless and sulfur-free fireworks shell lift-off agent, the quality of each component of the formula is:

[0027]

[0028] A smokeless and sulfur-free fireworks bomb lift-off agent, the specific steps are as follows:

[0029] Weigh 150 g of nitrocellulose, 25 g of dicyandiamide, 10 g of sepiolite fiber powder, 50 g of titanium hydride powder, 12.5 g of red rare earth photoluminescent powder, and 2.5 g of polyurethane adhesive according to the formula ratio.

[0030] The polyurethane adhesive was divided into three parts, the first part was 0.16g, the second part was 0.24g, and the third part was 2.1g.

[0031] Dissolve dicyandiamide in hot water at 60°C to prepare a dicyanamide solution, put it into a watering can, and spray it on the evenly spread sepiolite fiber powder; while spraying, turn the sepiolite fiber powder to ensure uniform spraying After the spraying is completed, place it in an oven at 120°C for 4 hours in vacuum, add the first part of polyurethan...

Embodiment 2

[0036] A smokeless and sulfur-free fireworks shell lift-off agent, the quality of each component of the formula is:

[0037]

[0038] A smokeless and sulfur-free fireworks bomb lift-off agent, the specific steps are as follows:

[0039] Weigh 370g of nitrocellulose, 111g of dicyandiamide, 59.2g of sepiolite fiber powder, 185g of titanium hydride powder, 74g of bright yellow rare earth photoluminescent powder, and 14.8g of polyurethane adhesive according to the formula ratio.

[0040] The polyurethane adhesive was divided into three parts, the first part was 0.6g, the second part was 1.2g, and the third part was 13g.

[0041] Dissolve dicyandiamide in hot water at 60°C to prepare a dicyanamide solution, put it into a watering can, and spray it on the evenly spread sepiolite fiber powder; while spraying, turn the sepiolite fiber powder to ensure uniform spraying After the spraying is completed, place it in an oven at 120°C for 4 hours in vacuum, add the first part of polyure...

Embodiment 3

[0046] A smokeless and sulfur-free fireworks shell lift-off agent, the quality of each component of the formula is:

[0047]

[0048]

[0049] A smokeless and sulfur-free fireworks bomb lift-off agent, the specific steps are as follows:

[0050] Weigh 1.6 kg of nitrocellulose, 1.2 kg of dicyandiamide, 0.2 kg of sepiolite fiber powder, 0.6 kg of titanium hydride powder, 0.28 kg of blue rare earth photoluminescent powder, and 0.12 kg of polyurethane adhesive according to the formula ratio.

[0051] The polyurethane adhesive was divided into three portions, the first portion was 5.7 g, the second portion was 4.3 g, and the third portion was 110 g.

[0052] Dissolve dicyandiamide in hot water at 60°C to prepare a dicyanamide solution, put it into a watering can, and spray it on the evenly spread sepiolite fiber powder; while spraying, turn the sepiolite fiber powder to ensure uniform spraying ; After the spraying is completed, place it in an oven at 120°C for 4 hours in vac...

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Abstract

The invention relates to a smokeless sulfur-free display shell lift-off agent and a preparation method thereof, and belongs to the technical field of civil entertainment fireworks. The method is as follows: weighing nitrocellulose, dicyandiamide, sepiolite fiber powder, titanium hydride powder, rare earth photoluminescence powder and a polyurethane adhesive; dividing the polyurethane adhesive intothree parts dissolving the dicyandiamide in hot water to prepare a dicyandiamide solution, spraying the dicyandiamide solution onto the sepiolite fiber powder, simultaneously stirring and drying thesepiolite fiber powder, dropwise adding a first part of polyurethane adhesive into the sepiolite fiber powder, grinding and sieving to obtain dicyandiamide / sepiolite fiber powder; mixing the titaniumhydride powder and the rare earth photoluminescence powder, dropwise adding a second part of polyurethane adhesive, sieving and drying to obtain the light-emitting granulation powder; and mixing the nitrocellulose, the dicyandiamide / sepiolite fiber powder and the light-emitting granulation powder, dropwise adding a third part of polyurethane adhesive, kneading, drying, grinding, sieving and granulating to obtain the smokeless sulfur-free display shell lift-off agent. The smokeless sulfur-free display shell lift-off agent provided by the invention has the advantages of good stability, low costand green and environment-friendly setting-off process.

Description

technical field [0001] The invention relates to a smokeless and sulfur-free fireworks shell lift-off agent and a preparation method thereof, belonging to the technical field of civilian entertainment pyrotechnics. Background technique [0002] Firework bombs are one of the most popular types of fireworks. In large-scale performances, they play an important role in exaggerating the joyful atmosphere. After launching into the air, they will show a variety of flower patterns and amazing effects. Greatly meet people's viewing needs. [0003] However, traditional fireworks bombs are now facing a severe development dilemma. Because their main component is black powder, which has poor stability, safety accidents occur frequently when fireworks bombs are set off, causing great losses to people's property and life safety. At the same time, the fireworks bombs produced serious dust and pungent smell during the discharge process, which polluted our living environment and went against ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C06B27/00C06B23/00
CPCC06B23/009C06B27/00
Inventor 刘吉平阮方于保藏李琪军刘克普吉伟生周耀明
Owner 江西吉润花炮新材料科技有限公司
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