Preparation method of fireproof flame-retardant wood
A fire retardant and wood technology, applied in the direction of wood treatment, wood impregnation, wood impregnation, etc., can solve the problems of low fire prevention effect, moisture absorption and exudation, etc., to achieve suitable promotion, delay heat transfer, wood flame retardant good performance
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Embodiment 1
[0022] A method for preparing fire-resistant and flame-retardant wood, said method comprising the following steps:
[0023] S1. Soak hydrotalcite in acid solution, heat to 50°C and keep for 10h, then wash with deionized water, and dry to obtain acidified hydrotalcite; the volume ratio of the hydrotalcite to the acid solution is 1:50, so Said acid solution is 40% dilute hydrochloric acid or nitric acid solution;
[0024] S2, described acidified hydrotalcite and graphite in the ball mill tank, then pass into carbon dioxide in the ball mill tank to get rid of the air therein, seal the ball tank, and then 30 Grinding at a speed of 0r / min for 6h to obtain modified hydrotalcite; the mass ratio of the acidified hydrotalcite to graphite is 100:1;
[0025] S3. Mix polyvinyl alcohol and nano silicon dioxide evenly, add acetic acid and stir evenly, then add triethanolamine and tetrabutyl titanate dropwise while stirring, and continue stirring for 1 hour after the addition is completed, ...
Embodiment 2
[0031] A method for preparing fire-resistant and flame-retardant wood, said method comprising the following steps:
[0032] S1. Soak hydrotalcite in acid solution, heat to 60°C and keep for 5h, then wash with deionized water, and dry to obtain acidified hydrotalcite; the volume ratio of the hydrotalcite to the acid solution is 1:100, so Said acid solution is 40% dilute hydrochloric acid or nitric acid solution;
[0033] S2. Put the acidified hydrotalcite and graphite in a ball mill tank, then introduce carbon dioxide into the nodular ink tank to get rid of the air therein, seal the nodular ink tank, and then grind at a speed of 600r / min for 1h to obtain modified hydrotalcite; The mass ratio of acidified hydrotalcite and graphite is 200:1;
[0034] S3. Mix polyvinyl alcohol and nano silicon dioxide evenly, add acetic acid and stir evenly, then add triethanolamine and tetrabutyl titanate dropwise while stirring, and continue stirring for 2 hours after the addition is completed,...
Embodiment 3
[0040] A method for preparing fire-resistant and flame-retardant wood, said method comprising the following steps:
[0041] S1. Soak the hydrotalcite in the acid solution, heat to 55°C and keep it for 6h, then wash with deionized water and dry to obtain the acidified hydrotalcite; the volume ratio of the hydrotalcite to the acid solution is 1:60, so Said acid solution is 40% dilute hydrochloric acid or nitric acid solution;
[0042] S2. Put the acidified hydrotalcite and graphite in a ball mill tank, then introduce carbon dioxide into the nodular ink tank to get rid of the air therein, seal the nodular ink tank, and then grind at a speed of 400r / min for 4h to obtain modified hydrotalcite; The mass ratio of acidified hydrotalcite and graphite is 180:1;
[0043] S3. Mix polyvinyl alcohol and nano silicon dioxide evenly, add acetic acid and stir evenly, then add triethanolamine and tetrabutyl titanate dropwise while stirring, and continue stirring for 1.5h after the dropwise add...
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