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A kind of polyvinyl chloride auxiliary heat stabilizer and preparation method thereof

A technology of auxiliary heat stabilizer and polyvinyl chloride is applied in the field of auxiliary heat stabilizer of polyvinyl chloride and its preparation, and can solve the problems of limited application range, high cost, and stability that cannot meet application requirements.

Active Publication Date: 2022-03-01
ANHUI JIAXIAN FUNCTIONAL AUXILIARY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, lead salts and cadmium soaps in metal soaps have good thermal stability, but due to toxicity problems, the application range is limited; organotin has excellent thermal stability and transparency, but the cost is high; most metal soaps are cheap , but the stability cannot meet the application requirements

Method used

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  • A kind of polyvinyl chloride auxiliary heat stabilizer and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] A polyvinyl chloride auxiliary heat stabilizer, comprising component A, component B and modified hydrotalcite;

[0035] This polyvinyl chloride auxiliary heat stabilizer is prepared through the following steps:

[0036]The first step, preparing component A and component B;

[0037] Second step, prepare modified hydrotalcite;

[0038] The third step is to mix component A and component B according to the weight ratio of 1:1 to obtain the first component, and then to mix the modified hydrotalcite and stearic acid according to the mass ratio of 1:1 to obtain the second component. The two components and the first component are mixed according to the mass ratio of 7:1 to obtain a polyvinyl chloride auxiliary heat stabilizer.

[0039] Wherein, preparation component A comprises the steps:

[0040] Step A11, add xylene, methyl stearate and sodium methoxide into a four-necked flask, set the temperature to 140°C, and the rotation speed to 300r / min, add acetophenone dropwise whi...

Embodiment 2

[0052] A polyvinyl chloride auxiliary heat stabilizer, comprising component A, component B and modified hydrotalcite;

[0053] This polyvinyl chloride auxiliary heat stabilizer is prepared through the following steps:

[0054] The first step, preparing component A and component B;

[0055] Second step, prepare modified hydrotalcite;

[0056] The third step is to mix component A and component B according to the weight ratio of 1:1 to obtain the first component, and then to mix the modified hydrotalcite and stearic acid according to the mass ratio of 1:2 to obtain the second component. The two components and the first component are mixed according to the mass ratio of 8:1 to obtain a polyvinyl chloride auxiliary heat stabilizer.

[0057] Wherein, preparation component A comprises the steps:

[0058] Step A11, add xylene, methyl stearate and sodium methoxide into a four-necked flask, set the temperature to 140°C, and the rotation speed to 300r / min, add acetophenone dropwise wh...

Embodiment 3

[0070] A polyvinyl chloride auxiliary heat stabilizer, comprising component A, component B and modified hydrotalcite;

[0071] This polyvinyl chloride auxiliary heat stabilizer is prepared through the following steps:

[0072] The first step, preparing component A and component B;

[0073] Second step, prepare modified hydrotalcite;

[0074] The third step is to mix component A and component B according to the weight ratio of 1:1 to obtain the first component, and then to mix the modified hydrotalcite and stearic acid according to the mass ratio of 1:3 to obtain the second component. The two components and the first component are mixed according to the mass ratio of 9:1 to obtain a polyvinyl chloride auxiliary heat stabilizer.

[0075] Wherein, preparation component A comprises the steps:

[0076] Step A11, add xylene, methyl stearate and sodium methoxide into a four-necked flask, set the temperature to 140°C, and the rotation speed to 300r / min, add acetophenone dropwise wh...

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Abstract

The invention discloses a polyvinyl chloride auxiliary heat stabilizer and a preparation method thereof, comprising component A, component B and modified hydrotalcite; the polyvinyl chloride auxiliary heat stabilizer is prepared through the following steps: the first step, preparation group Divide A and B; the second step is to prepare modified hydrotalcite; the third step is to mix component A and component B according to the weight ratio of 1:1 to obtain the first component, and then the modified hydrotalcite and hard Fatty acid is mixed according to the mass ratio of 1:1-3 to obtain the second component, and the second component and the first component are mixed according to the mass ratio of 7-9:1 to obtain a polyvinyl chloride auxiliary heat stabilizer, modified When hydrotalcite is added to the synthesis process of polyvinyl chloride, due to dehydration, the hydrogen bonds of the sheets disappear, and the sheets are free, which reduces the bubbles generated during the preparation of polyvinyl chloride products. The prepared component A and component B are the same as the modified It is combined with non-toxic hydrotalcite to achieve auxiliary thermal stabilization effect.

Description

technical field [0001] The invention belongs to the technical field of preparation of plastic additives, and in particular relates to a polyvinyl chloride auxiliary heat stabilizer and a preparation method thereof. Background technique [0002] Polyvinyl chloride has excellent corrosion resistance and high mechanical properties, and is cheap, rich in resources, and mature in manufacturing technology, so its products are widely used in various fields of industrial and agricultural production. However, because the polyvinyl chloride structure contains double bonds, branched chain structures and initiator residues, etc., it degrades with the dehydrochlorination reaction at the processing temperature, and also undergoes discoloration and macromolecular crosslinking. Therefore, heat stabilizers must be used in the processing of polyvinyl chloride. For a long time, the heat stabilizers used for PVC mainly include lead salts, composite metal soaps and organotins. Among them, lead...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L27/06C08K5/09C08K3/26C08K9/04C08K5/29C08K13/06
CPCC08K5/09C08K3/26C08K9/04C08K5/29C08K13/06C08L2201/08C08L27/06
Inventor 张忠洁李兑黄先胜李平童庆军
Owner ANHUI JIAXIAN FUNCTIONAL AUXILIARY
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