Device and method for synthesizing and purifying macamides

Abstract

The invention discloses a device and a method for synthesizing and purifying macamides, which relate to the technical field of biological pharmacy, and aim to solve the problems that in the prior art, macamides need to be purified, cooled and crystallized in the process of synthesizing the macamides, but a natural cooling mode is usually adopted for crystallization at present, the cooling speed is slow, and the crystallization efficiency is low. A supporting plate is fixedly mounted above the working bottom plate, a synthesis box is fixedly mounted above the supporting plate, a filtering box is arranged below the synthesis box along one side of the supporting plate, a purifying box is arranged below the filtering box, and the purifying box is fixedly connected with the working bottom plate through bolts; a liquid scattering assembly is arranged in the purifying box, the liquid scattering assembly is composed of an upper plate, a vertical plate and a lower plate, the upper plate is arranged above the vertical plate, and the vertical plate is arranged above the lower plate.

Description

technical field [0001] The invention relates to the technical field of biopharmaceuticals, in particular to a device and method for synthesizing and purifying macamide. Background technique [0002] Maca amide compounds are the amide alkaloids with the least basicity among nitrogen-containing alkaloids. In maca, macamide is biotransformed from benzylamine and fatty acid molecules, and has a long carbon chain and With multiple degrees of unsaturation, Maca is a genus of Brassicaceae. It has thousands of years of edible history and a wide range of biological effects. However, the growth environment of Maca is harsh, the yield is low, and the content of macamide in Maca is extremely low. , and the components in maca are complex, so that using maca as raw material, the method of biochemical separation and preparation of macamide is limited by the difficulty of separation and purification, the limitation of raw material sources, and the inability to prepare on a large scale. Howe...

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Problems solved by technology

[0004] The object of the present invention is to provide a kind of device and method for synthesizing and purifying macamide, in order to solve the process of synthesizing macamide proposed in the above-mentioned background technology, it is necessary to purify and cool down crystallization of macamide, but natural Crystallization is carried out by cooling and cooling, the cooling speed is slow, and the crystallization efficiency is low

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