Formoterol/steroid bronchodilating compositions and methods of use thereof
a technology of bronchodilating compositions and steroid, which is applied in the direction of drug compositions, inorganic non-active ingredients, dispersed delivery, etc., can solve the problems of insufficient stability of compounds such as formoterol, which has many desirable properties, and is difficult to administer in liquid form
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example 1
Preparation of Solution Formulations
[0099]Polyethylene glycol 400 and / or propylene glycol and vitamin E TPGS were mixed in a stainless steel container with heating at about 42° C. until a homogeneous liquid formed. While maintaining the liquid phase, the temperature was lowered and the steroid active ingredient, e.g., budesonide or fluticasone propionate, was added. The mixing was continued until all of the drug substance had dissolved. In another container all other ingredients, including formoterol fumarate dihydrate, were mixed with about 70% water until a clear solution formed. The two solutions were mixed together until a homogeneous clear solution formed. The volume Was made up with water and the solution was mixed to give the desired composition.
[0100]Using the above procedure, the following solution compositions containing the indicated ingredients in the indicated amounts were prepared. For each steroidal anti-inflammatory agent, a low strength and a high strength formulati...
example 2
Preparation of Suspension Formulations
[0101]All ingredients, with the exception of formoterol fumarate dihydrate and the steroidal anti-inflammatory agent, e.g., budesonide or fluticasone propionate, were dissolved in about 40% water in a container with mixing. The steroidal active ingredient was added and the mixture was dispersed with high speed homogenization. Formoterol fumarate dihydrate was dissolved in about 50% water with mixing and the resulting solution was added to the steroidal suspension with mixing until a uniform suspension formed.
[0102]Using the above procedure, the following suspension formulations containing the indicated ingredients in the indicated amounts were prepared.
Budesonide / Formoterol suspension formulationsIngredientConcentrationFormoterol fumarate dihydrate5-2000 μg / mL or 50-200 μg / mLBudesonide125-500μg / mLDisodium edetate0.1-0.2mg / mLPolysorbate 800.2-0.3mg / mLSodium chloride5-10mg / mLCitrate buffer1-20mMWaterq.s.
Fluticasone propionate / Formoterol suspension...
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