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1 results about "Graphite furnace atomic absorption" patented technology

Graphite furnace atomic absorption spectroscopy (GFAAS) (also known as Electrothermal Atomic Absorption Spectroscopy (ETAAS)) is a type of spectrometry that uses a graphite-coated furnace to vaporize the sample. Briefly, the technique is based on the fact that free atoms will absorb light at frequencies or wavelengths characteristic of the element of interest (hence the name atomic absorption spectrometry). Within certain limits, the amount of light absorbed can be linearly correlated to the concentration of analyte present. Free atoms of most elements can be produced from samples by the application of high temperatures. In GFAAS, samples are deposited in a small graphite or pyrolytic carbon coated graphite tube, which can then be heated to vaporize and atomize the analyte. The atoms absorb ultraviolet or visible light and make transitions to higher electronic energy levels. Applying the Beer-Lambert law directly in AA spectroscopy is difficult due to variations in the atomization efficiency from the sample matrix, and nonuniformity of concentration and path length of analyte atoms (in graphite furnace AA). Concentration measurements are usually determined from a working curve after calibrating the instrument with standards of known concentration. The main advantages of the graphite furnace comparing to aspiration atomic absorption are the following...

Method for the preparation of 7-(5-nitro-4-methyl-2-pyridylazo)-8-hydroxyquinoline and its use in the detection of trace amounts of platinum

PendingCN122277527AQuinolineIonic liquid
This invention discloses a method for preparing 7-(5-nitro-4-methyl-2-pyridineazo)-8-hydroxyquinoline and its application in the detection of trace platinum. The preparation method includes the following steps: (1) preparing 5-nitro-4-methyl-2-aminopyridine diazonium salt; (2) preparing 7-(5-nitro-4-methyl-2-pyridineazo)-8-hydroxyquinoline. 7-(5-nitro-4-methyl-2-pyridineazo)-8-hydroxyquinoline, as a chelating agent, reacts with platinum in water to form a hydrophobic chelate. Then, ionic liquid extraction is used. The extract phase does not need to be diluted and can be directly used for the determination of platinum in water by graphite furnace atomic absorption spectrometry. This solves the defects of ionic liquids, which are viscous and difficult to transfer directly or easily adsorbed on instrument components. The operation steps are simplified by eliminating the need for dilution. At the same time, the detection method provided by this invention is convenient to operate and has high precision.
Owner:XIAN UNVERSITY OF ARTS & SCI