This invention discloses a method for preparing 7-(5-nitro-4-methyl-2-pyridineazo)-8-hydroxyquinoline and its application in the detection of trace
platinum. The preparation method includes the following steps: (1) preparing 5-nitro-4-methyl-2-aminopyridine diazonium salt; (2) preparing 7-(5-nitro-4-methyl-2-pyridineazo)-8-hydroxyquinoline. 7-(5-nitro-4-methyl-2-pyridineazo)-8-hydroxyquinoline, as a chelating agent, reacts with
platinum in water to form a hydrophobic chelate. Then,
ionic liquid extraction is used. The extract phase does not need to be diluted and can be directly used for the determination of
platinum in water by
graphite furnace atomic absorption spectrometry. This solves the defects of ionic liquids, which are viscous and difficult to transfer directly or easily adsorbed on instrument components. The operation steps are simplified by eliminating the need for
dilution. At the same time, the detection method provided by this invention is convenient to operate and has high precision.