Filtrate reducer for oil field well drilling fluid

A fluid loss reducer, oil field drilling technology, applied in drilling compositions, chemical instruments and methods, etc., can solve the problems of irreversible degradation, reduction in efficiency, inability to function, etc.

Active Publication Date: 2007-10-17
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, field use shows that iron-chromium salts will lose their effectiveness at temperatures above 130°C, and irreversible degradation will occur when the temperature exceeds 177°C
Therefore the synergistic effect of sulfomethyl lignite and lignosulfonate is limited
Especially in the case of high temperature and high salt, the two will not be able to play a role due to their own shortcomings.

Method used

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  • Filtrate reducer for oil field well drilling fluid

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0039] Get 100 grams of sulfomethyl lignite, dissolve in water, add 10 grams of sodium lignosulfonate, 3 grams of dimethyl diallyl ammonium chloride, 0.01 gram of ferric chloride (FeCl 3 ), and stir well.

[0040] Pour the solution into the reaction kettle (or directly mix in the reaction kettle), turn on the stirring, and react at 150°C for 2 hours, and the pressure is normal pressure. After the reaction, the product is a black liquid, and the product 1# is obtained after evaporating the water. The product is a black powder with good water solubility.

example 2

[0042] Take 100 grams of sulfomethyl lignite, dissolve it in water, add 25 grams of sodium lignosulfonate, 10 grams of dimethyl diallyl ammonium chloride, and 0.05 grams of ferric chloride, and stir evenly.

[0043] Pour the solution into the reaction kettle (or directly mix in the reaction kettle), turn on the stirring, and react at 120°C for 4 hours, and the pressure is normal pressure. After the reaction, the obtained product is a black liquid, and the product is obtained after evaporating the water. The product is black powder 2# and has good water solubility.

example 3

[0045] Take 100 grams of sulfomethyl lignite, dissolve it in water, add 50 grams of sodium lignosulfonate, 15 grams of dimethyl diallyl ammonium chloride, and 0.52 grams of ferric chloride, and stir evenly.

[0046] Pour the solution into the reaction kettle (or directly mix in the reaction kettle), turn on the stirring, and react at 85° C. for 6 hours, and the pressure is normal pressure. After the reaction, the obtained product is a black liquid, and the product is obtained after evaporating the water. The product is a black powder 3# with good water solubility.

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Abstract

The invention relates to an oil field fluid loss additive for drilling liquid and its producing method and the application of the treating agent in the process of producing drilling liquid system. The treating agent utilizes the cation monomer dimethyl diallyl ammonium chloride can make the sodium lignin sulfonate and the sulfonated-methyl brown coal graft induced by FeCl3 so as to produce a new fluid loss agent with the resistance to salt and collapse at high temperature. The composed product integrates the brown coal and lignin. The cation introduction improves the resistance to collapse. The weak crosslinking function of the Fe3+ makes the heat resistance improved further based on the brown coal. Therefore, the product can be widely applied in different complicated conditions such as high temperature deep well, gypsum/slat bed, stratum with a bad water sensitivity, fragility stratum and etc. and has a good prospect.

Description

technical field [0001] The invention relates to an additive for oilfield drilling fluid, more specifically, to a fluid loss reducer for oilfield drilling fluid. The treatment agent has the ability to resist high temperature and salt intrusion. technical background [0002] In oil drilling operations, when the drilling fluid flows through the permeable formation under pressure, it will infiltrate, causing the liquid phase of the drilling fluid to infiltrate into the formation. This process is collectively called "water loss". If water loss cannot be well controlled, a large amount of water loss entering the formation will not only induce wellbore instability, but also cause damage to oil and gas formations. At present, the effective way to solve this problem is to add fluid loss control agent in the drilling fluid. [0003] The fluid loss control agents used in oilfield drilling fluid mainly include the following types: [0004] (1) Special ultrafine particle materials, suc...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/035
Inventor 赵素丽常连玉肖超江山红李娟蔡利山王治法谭春勤徐江
Owner CHINA PETROLEUM & CHEM CORP
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