Quality inspection method of cough pills

A quality inspection method and technology for Zhike Pills, which are applied in the field of quality inspection of Zhike Pills, can solve problems such as difficulty in accurately controlling the quality of Zhike Pills, large limitations, etc., and achieve the effect of improving quality control standards and high-quality standards.

Active Publication Date: 2011-08-17
KUNMING CHINESE MEDICINE FACTORY
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Problems solved by technology

The eleventh volume of "Drug Standards of the Ministry of Health of the People's Republic of China" promulgated the quality control standards for cough pills (WS 3 -B-2096-96), but in the existing quality control methods of cough pills issued by the Ministry of Health, there are only microscopic identification and physical and chemical reaction identification, which has great limitations and is difficult to accurately control the quality of cough pills

Method used

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Embodiment

[0019] The formula of the cough pill is: 20g of ephedra, 40g of perilla seed, 50g of Magnolia officinalis (Ginger Sunburn), 20g of Tinglizi, 4g of Chuan Fritillaria, 20g of French pinellia (stir-fried with sand), 18g of ginkgo, 50g of poppy shell, borax 6g, Citrus aurantium (stir-fried bran) 40g, Chenpi 70g, Bellflower 30g, Fangfeng 40g, Poria cocos 70g, Baiqian 20g, Peucedanum 30g, licorice 40g, mulberry leaves 50g, Scutellaria baicalensis (wine-roasted) 10g, Nansha ginseng 60g, mint 50g , perilla leaves 40g. Preparation method: decoct mulberry leaves, poppy shells, and licorice twice with water for the above twenty-two flavors, 2 hours each time, combine the decoction, filter, concentrate the filtrate to an appropriate amount, add borax to dissolve; Bawei is crushed into fine powder, sieved, mixed evenly, pilled with the above-mentioned concentrated medicinal solution, dried, coated with sugar, and obtained. Properties: This product is a sugar-coated concentrated pill, whic...

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Abstract

The invention relates to a quality inspection method of cough pills prescribed in Volume 11 of Drug Standard of Ministry of Public Health of the People's Republic of China (Chinese Traditional Patent Formulation Preparations). The quality inspection method comprises microscopic identification of cough pills, a thin-layer chromatography identification method of ephedrine hydrochloride, magnolol and dried orange peel, a thin-layer chromatography qualitative identification method of bitter orange and a content determination method of ephedrine hydrochloride in the cough pills. The quality inspection method raises the quality control standards of cough pills and establishes content determination inspection indexes of main drugs in a preparation and a inspection method thereof; and meanwhile, the quality inspection method deletes physical and chemical reaction identification of poor specialization and adds the thin-layer chromatography qualitative identification method of ephedrine hydrochloride, magnolol, dried orange peel and bitter orange, thereby ensuring a higher quality standard level of compound preparations of cough pills.

Description

technical field [0001] The invention relates to a quality detection method for cough pills in Volume 11 of "Drug Standards of the Ministry of Health of the People's Republic of China" (preparations of traditional Chinese medicine). Background technique [0002] Drug cough pills (WS 3 -B-2096-96), has the effect of lowering qi and resolving phlegm, relieving cough and relieving asthma. It is used for cough with excessive phlegm, shortness of breath, chest tightness, body aches or chronic cough caused by wind-cold entering the lungs and stagnant lung qi, and elderly acute Chronic bronchitis. The compound preparation consists of 20g of Chinese medicine ephedra, 40g of perilla seed, 50g of Magnolia officinalis (Ginger Sunburn), 20g of Tinglizi, 4g of Chuan Fritillaria, 20g of French pinellia (stir-fried with sand), 18g of ginkgo, 50g of poppy shell, 6g of borax, Fructus aurantii (stir-fried with bran) 40g, orange peel 70g, bellflower 30g, windproof 40g, poria cocos 70g, white ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N30/36A61K36/8966A61K33/22A61K9/20A61P11/14A61P11/10A61P11/06A61P11/00
Inventor 张兴元田婷婷朱敏
Owner KUNMING CHINESE MEDICINE FACTORY
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