Method for detecting cement dosage in core test sample of cement mixing pile

A technology of cement mixing pile and detection method, which is applied in the direction of chemical analysis by titration method, can solve the problems of difficulty in grasping the accuracy, great influence of experimental results, and influence on Ca2+ dissolution rate, etc., to achieve elimination of influence and high accuracy Effect

Inactive Publication Date: 2011-03-02
HOHAI UNIV
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Problems solved by technology

[0005] (1) The operation specification of EDTA titration stipulates that the variation range of moisture content of the sample is 2%, but the variation range of moisture content in the core sample of cement mixing pile sometimes reaches 15%, which does not meet the requirements of the specification
[0006] (2) Due to the differences in sample preparation methods and curing conditions will affect the various processes of cement hydrolysis, hydration and coagulation hardening, indirectly affect the dissolution rate of Ca2+ in NH4Cl solution, thus affecting the amount of EDTA disodium standard solution during detection
[0007] (3) "Code for Testing of Highway Inorganic Binder Stable Materials" (JTJ057-94) stipulates that it is not affected by the age of cement and lime stabilized soil (within 7d), and the accuracy of detection after 7d is difficult to grasp
The cement mixing pile can only be drilled and cored for inspection after 28 days after the construction is completed. Through experiments, it is found that the influence of age has a great influence on the experimental results

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  • Method for detecting cement dosage in core test sample of cement mixing pile
  • Method for detecting cement dosage in core test sample of cement mixing pile
  • Method for detecting cement dosage in core test sample of cement mixing pile

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Embodiment 8

[0049] The present invention adopts standard sample comparison method, prepares and maintains samples by simulating on-site pile body preparation and maintenance conditions, studies the attenuation law of each cement dosage sample with age to obtain standard curves at different ages, and uses different age standards by analyzing Curve to detect the accuracy of the cement dosage of the same sample, and the standard curve of the corresponding age should be used for the detection of samples of different ages. image 3 It is the standard curve of EDTA consumption versus age versus cement dosage for ages 7d, 14d, 28d, 35d, 49d and 90d, referring to image 3 , it can be seen that different ages have a great influence on the measurement results of the cement dosage of the samples. Taking the standard curve with an age of 28 days as an example, the EDTA consumption of the sample with a cement dosage of 25% is 26.0mL, and according to the consumption of EDTA, different ages can be found ...

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Abstract

The invention discloses a method for detecting cement dosage in a core test sample of a cement mixing pile, which comprises the following steps: directly mixing a field in-situ soil sample with water content without major changes into cement slurry with the same water-cement ratio during field construction, and preparing the test sample into the standard cylindrical test sample with unconfined compressive strength; placing the test sample in same-level in-situ plain soil for extrusion, sealing and maintenance after molding; carrying out EDTA titration after achieving the preset age, obtaining an attenuation law curve of consumption of disodium EDTA along with the age, and establishing standard curves in all the ages according to the attenuation law curve; and determining the consumption of EDTA in the sample, checking the cement dosage from the standard curve, and finally obtaining the cement dosage in the core test sample of the cement mixing pile. The method has simple operation, accurate detection result, good stability and good repeatability.

Description

technical field [0001] The invention belongs to the intersecting field of basic geotechnical experiment of geotechnical engineering and material engineering dosage detection, and in particular relates to an improved EDTA titration method for cement dosage of a cement mixing pile coring sample. Background technique [0002] The current inspection method of cement mixing piles mainly includes two aspects: one is the sensory inspection of piles, that is, about 7 days after pile formation, the sensory inspection of piles is carried out by detecting the number of piles, the distance between piles, and the pile position. The second is the detection of the quality of the pile body itself, which is divided into the integrity of the pile body, the overall size of the pile body, the uniformity, the compactness, the continuity of the pile body, the strength and the bearing capacity of a single pile. Among them, the quality uniformity detection of the deep mixing pile is judged by visua...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N31/16
Inventor 张福海杨立国佟宏伟丰土根李玉龙刘浔吕子鑫王磊
Owner HOHAI UNIV
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