Synchronization acquisition method of active phosphorus and iron in deposit
A simultaneous acquisition and sedimentation technology, which is applied in the preparation of test samples, measurement of color/spectral characteristics, and material analysis by observing the influence of chemical indicators, etc., can solve the difficulties of investigation, high cost, and low acquisition efficiency, etc. problem, to achieve the effect of short acquisition time, simple operation procedure and high efficiency
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[0042] Below in conjunction with accompanying drawing and example the method of the present invention is further described.
[0043] Put the DGT device in the method of the present invention into the Meiliang Bay sediment in Taihu Lake, take it out after 48 hours, transport it back to the laboratory, analyze the phosphorus and iron on the fixed film, and convert the phosphorus and iron accumulation on the fixed film Obtain the content and spatial distribution of reactive phosphorus and iron in sediment profiles.
[0044] The concrete operation of described method comprises the following steps:
[0045] (1) Preparation of phosphorus-iron synchronous enrichment fixed membrane: Mix 1g of hydrated zirconium hydroxide powder with a moisture content of 50±5% and 3-5mL of 30% polyacrylamide aqueous solution, grind, add 0.6-1g Chelex-100 cation exchange Stir the resin evenly to obtain a film-forming solution; add 4-8 μL of tetramethyldiethylamine (TEMED) and 12-16 μL of 10% (wt) ammo...
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