Complete organic and inorganic explosive analyser
A comprehensive analysis and explosives technology, applied in the analysis of materials, material analysis by electromagnetic means, instruments, etc., can solve the problems of low ionization efficiency, improve selectivity and specificity, facilitate qualitative analysis, and improve ionization efficiency and the effect of detection sensitivity
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Embodiment 1
[0019] The thermal analysis sampler 1 uses the halogen beam heating lamp LCB-50 to heat the sample non-contact, and the distance between the heating lamp and the sampling cloth 4 is 35 mm.
[0020] The carrier gas flows in from the carrier gas inlet 2 of the thermal analysis injector 1, and the sample molecules flow out from the sample gas outlet 3; the carrier gas is pure dry air, and the carrier gas flow rate is 100-500mL / min.
[0021] A nickel source 5 is provided on the gas path at the rear end of the sample gas outlet 3 of the thermal analysis injector 1; the distance between the nickel source 5 and the sample gas outlet 3 is 15 mm.
[0022] A low-temperature plasma ionization source 6 is arranged on the gas path at the rear end of the nickel source 5; the distance between the low-temperature plasma ionization source 6 and the nickel source 5 is 10 mm. The low-temperature plasma ionization source 6 uses a glass tube with an outer diameter of 6 mm and a thickness of 1 mm a...
Embodiment 2
[0025] The thermal analysis sampler 1 conducts contact heating on the sample through a hot stainless steel metal block.
[0026] The carrier gas flows in from the carrier gas inlet 2 of the thermal analysis injector 1, and the sample molecules flow out from the sample gas outlet 3; the carrier gas is pure dry air, and the carrier gas flow rate is 100-500mL / min, which can be selected in the air Add dichloromethane, O 3 Such doping gases can improve the selectivity and specificity of explosive detection.
[0027] A nickel source 5 is provided on the gas path at the rear end of the sample gas outlet 3 of the thermal analysis injector 1; the distance between the nickel source 5 and the sample gas outlet 3 is 15 mm.
[0028] A nickel source 5 is provided on the gas path at the rear end of the sample gas outlet 3 of the thermal analysis injector 1; the distance between the nickel source 5 and the sample gas outlet 3 is 15 mm.
[0029] A low-temperature plasma ionization source 6 i...
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