Seabuckthorn flavone extraction method and seabuckthorn flavone extract
A seabuckthorn flavonoid and an extraction method technology are applied to the extraction of seabuckthorn flavonoids and the field of seabuckthorn flavonoid extracts, which can solve the problems of low content of active ingredients, inconvenient taking, large dosage for patients, etc., and achieve stable active ingredients and no damage to active ingredients. , the effect of simple structure
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Embodiment 1
[0021] Take 1000g seabuckthorn, add 10 times the weight of seabuckthorn medicinal materials in water, soak for 0.5h, decoct for 1 hour, filter, add 8 times the weight of medicinal materials in water, decoct for 1 hour, filter out the medicinal liquid, combine and decoct twice Liquid, concentrated to a relative density of 1.05 at 60°C, adding ethanol to make the volume percentage of the alcohol content reach 75%, stirring, standing, and filtering, the relative density of the filtrate was 1.25 when the filtrate was concentrated to 65°C, and the ethanol was recovered to obtain a concentrated solution. Use macroporous resin for refining, collect the eluent, continue to concentrate, and dry the concentrated solution to obtain seabuckthorn flavonoid extract.
[0022] The extraction method of seabuckthorn flavonoids, the purification method of the macroporous resin is: adding to a macroporous adsorption resin column, eluting with 50% ethanol, collecting 5 times the column volume eluat...
Embodiment 2
[0033] Take 1000g seabuckthorn, add 10 times the weight of seabuckthorn medicinal materials in water, soak for 0.5h, decoct for 1 hour, filter, add 8 times the weight of medicinal materials in water, decoct for 1 hour, filter out the medicinal liquid, combine and decoct twice Liquid, concentrated to a relative density of 1.05 at 60°C, adding ethanol to make the volume percentage of the alcohol content reach 75%, stirring, standing, and filtering, the relative density of the filtrate was 1.25 when the filtrate was concentrated to 65°C, and the ethanol was recovered to obtain a concentrated solution. Use macroporous resin for refining, collect the eluent, continue to concentrate, and dry the concentrated solution to obtain seabuckthorn flavonoid extract.
[0034] The extraction method of seabuckthorn flavonoids, the purification method of the macroporous resin is: adding to a macroporous adsorption resin column, eluting with 50% ethanol, collecting 5 times the column volume eluat...
Embodiment 3
[0038] Take 1000g seabuckthorn, add 10 times the weight of seabuckthorn medicinal materials in water, soak for 0.5h, decoct for 1 hour, filter, add 8 times the weight of medicinal materials in water, decoct for 1 hour, filter out the medicinal liquid, combine and decoct twice Liquid, concentrated to a relative density of 1.05 at 60°C, adding ethanol to make the volume percentage of the alcohol content reach 75%, stirring, standing, and filtering, the relative density of the filtrate was 1.25 when the filtrate was concentrated to 65°C, and the ethanol was recovered to obtain a concentrated solution. Use macroporous resin for refining, collect the eluent, continue to concentrate, and dry the concentrated solution to obtain seabuckthorn flavonoid extract.
[0039] The extraction method of seabuckthorn flavonoids, the purification method of the macroporous resin is: adding to a macroporous adsorption resin column, eluting with 50% ethanol, collecting 5 times the column volume eluat...
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