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Allspiceessential oil stage-extraction method and application of method in cigarettes

A technology of allspice essential oil and extraction method, which is applied in the direction of essential oil/fragrance, application, tobacco, etc., to achieve the effect of high yield and reasonable design of process parameters

Inactive Publication Date: 2016-12-14
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] And the extraction and application of pimento essential oil have not yet been reported in cigarettes, therefore, it is very meaningful to provide a segmented extraction method of pimento quintessence oil and its application in cigarettes, and it is also necessary

Method used

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  • Allspiceessential oil stage-extraction method and application of method in cigarettes

Examples

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Effect test

Embodiment 1

[0024] A segmented extraction method of allspice essential oil, comprising the steps of:

[0025] 1) Put the dried allspice fruit and distilled water into a flask at a weight ratio of 1:18 and soak for 1 hour, then add glass beads into the flask, shake and mix; Tube;

[0026] 2) Heating distillation, the distillation time is 6h, the distillation temperature is 90°C, start timing from the distillation of the pimento essential oil, collect the oil-water mixture released from the volatile oil tester from the first hour to the end of the second hour, and let it stand Layering, collecting the allspice essential oil part, namely obtaining the allspice essential oil extracted in sections, which is recorded as allspice essential oil A.

[0027] An application of the allspice essential oil prepared by the above method in cigarettes comprises the following steps: taking the allspice essential oil A with a weight of 0.01% cut tobacco weight, diluting the allspice essential oil A with 5m...

Embodiment 2

[0029] A segmented extraction method of allspice essential oil, comprising the steps of:

[0030] 1) Put the dried allspice fruit and distilled water into a flask at a weight ratio of 1:22 and soak for 5 hours, then add glass beads to the flask, shake and mix; Tube;

[0031] 2) Heating distillation, the distillation time is 8h, and the distillation temperature is 85°C. Start timing from the distillation of the pimento essential oil, collect the oil-water mixture released from the volatile oil tester from the third hour to the end of the sixth hour, and let it stand Layering, collecting the allspice essential oil part, namely obtaining the allspice essential oil extracted in sections, which is recorded as allspice essential oil B.

[0032] An application of the allspice essential oil prepared by the above method in cigarettes, the allspice essential oil B with a weight of 0.1% cut tobacco weight is taken, the allspice essential oil B is diluted with 5mL70% ethanol, and the dil...

Embodiment 3

[0034] A segmented extraction method of allspice essential oil, comprising the steps of:

[0035] 1) Put the dried allspice fruit and distilled water into a flask at a weight ratio of 1:20 and soak for 2 hours, then add glass beads into the flask, shake and mix; Tube;

[0036] 2) Heating distillation, the distillation time is 8h, the distillation temperature is 90°C, start timing from the distillation of the pimento essential oil, collect the oil-water mixture released from the volatile oil tester from the first hour to the end of the second hour, and let it stand Layering, collecting the allspice essential oil part, namely obtaining the allspice essential oil extracted in sections, which is recorded as allspice essential oil A.

[0037] An application of the allspice essential oil prepared by the above method in cigarettes, the allspice essential oil A with a weight of 0.05% cut tobacco weight is taken, the allspice essential oil A is diluted with 5mL70% ethanol, and the dil...

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Abstract

The invention provides an allspiceessential oil stage-extraction method and application of the method in cigarettes. The allspiceessential oil stage-extraction method comprises the following steps that 1, dried allspice fruits and distilled water are put in a flask according to the weight ratio of 1: (18-22) for soaking, then glass beads are added to the flask, shaking and mixing are performed, and upper portion of the flask is connected with a volatile oil determinator and a reflux condensing tube; 2, heating distillation and stage-extraction are performed. The invention further provides application of allspiceessential oil prepared by adopting the method in cigarettes. The allspiceessential oil stage-extraction method is reasonable in parameter design and high in allspiceessential oil yield. The allspiceessential oil is applied to the cigarettes, can be harmonious with cigarette flavor, the smoke richness is slightly improved, the flavor quality is improved, the smoke is fine and smooth, the softness is better, the sweet taste is obvious, the flavor amount is reduced, and aftertasteis refreshing.

Description

technical field [0001] The invention relates to the technical field of tobacco essence and fragrance, in particular to a segmented extraction method of allspice essential oil and its application in cigarettes. Background technique [0002] Natural essential oils are called essential oils or essential oils in botany, aromatic oils in business, and volatile oils in chemistry and medicine. They exist in different tissues of plants such as fruits, An important class of secondary substances in leaves, flowers and roots, composed of simple compounds with small molecular weights, mostly oily liquids at room temperature, volatile, with strong fragrance and smell. They are often the essence of plant fragrance, generally a complex mixture of dozens to hundreds of compounds, and have strong biological activities in many aspects, and are an important chemical component contained in plants. [0003] The content of plant essential oils varies from 1% to 10%. The oil content is affected b...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24B3/12A24B15/24
CPCC11B9/027A24B3/12A24B15/241
Inventor 肜霖董世良熊国玺
Owner HUBEI CHINA TOBACCO IND
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