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A high temperature and high pressure multiphase flow dynamic visualization loop corrosion test device and method

A high-temperature, high-pressure, corrosion testing technology, applied in the direction of measuring devices, weather resistance/light resistance/corrosion resistance, instruments, etc., can solve the lack of shear force measurement devices, lack of real-time recording methods for experimental data, and inability to monitor surface corrosion of test pieces online issues such as occurrence and corrosion processes

Inactive Publication Date: 2018-08-10
SOUTHWEST PETROLEUM UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] (1) The method of stirring in the reactor is mainly used to simulate the corrosion effect of the flowing medium on the test piece, which cannot truly reflect the complex flow conditions and scouring effects of the multiphase flow medium in the pipeline;
[0006] (2) It is impossible to truly simulate the scouring damage effect of subcritical and supercritical fluids on the test piece;
[0007] (3) There is a lack of visualization devices, and there is little detailed research on the precipitation methods, conditions and forms of sulfur particles;
[0008] (4) Lack of shear force measurement device, unable to quantitatively analyze the erosion and damage effect of multiphase flow corrosion medium on corrosion inhibitor film and corrosion product film
[0009] (5) Lack of online corrosion detection means, unable to monitor the occurrence and process of corrosion on the surface of the test piece online;
[0010] (6) There is a lack of real-time recording means for experimental data, and relevant experimental data cannot be collected and processed in real time

Method used

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  • A high temperature and high pressure multiphase flow dynamic visualization loop corrosion test device and method
  • A high temperature and high pressure multiphase flow dynamic visualization loop corrosion test device and method
  • A high temperature and high pressure multiphase flow dynamic visualization loop corrosion test device and method

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Embodiment

[0061] Adopt the present invention to carry out experiment to multi-phase flow acidic corrosion medium to the corrosion of equipment and the destructive effect of scouring under different production working conditions, its experimental process is as follows:

[0062] Step 1: Install 1# curved test piece 34, 2# curved test piece 35, 3# curved test piece 36, 4# curved test piece 37 to corrosion test piece testing device 31, inductance resistance probe 50, reference After the comparison electrode 51, the working electrode 52 and the counter electrode 53 arrive at the electrochemical signal detection device 30, connect and install the medium displacement unit 58 and each element on the circulation loop 15, and perform debugging;

[0063] Step 2: Open 3# valve 3, N 2 Deoxygenation through booster pump 8, 4# valve 4, 5# valve 5, 1# high temperature autoclave body 9, 6# valve 6, 7# valve 7, intake valve 14, circulation loop 15, exhaust valve 19 , the time is 1h, then close the 3# valv...

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Abstract

The invention discloses a high-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus and a method thereof. The high-temperature and high-pressure multi-phase flow dynamic visualization loop corrosion testing apparatus comprises a medium displacement unit, an experiment parameter measurement unit, a visualization unit, a corrosion testing unit, a gas inlet valve, a circulation loop, a driving pump, a 1# end cover, a 2# end cover, a gas discharge valve and an H2S absorption device, wherein the experiment parameter measurement unit, the corrosion testing unit, the 1# end cover, the 2# end cover, the gas discharge valve and the H2S absorption device are arranged on the circulation loop, and the medium displacement unit is connected to the circulation loop through the driving pump. According to the present invention, the subcritical and supercritical fluids under the high-temperature and high-pressure environment can be realistically simulated, the shearing force can be measured, the erosion damage effect of the multi-phase flow corrosion medium on the corrosion inhibitor film and the corrosion product film can be quantitatively analyzed, and the online testing of the pipeline corrosion effect can be completed and the results are recorded.

Description

technical field [0001] The invention relates to a high-temperature and high-pressure multiphase flow dynamic visualization loop corrosion test device and method, and belongs to the technical field of petrochemical anticorrosion. Background technique [0002] With the continuous development of my country's oil and gas fields, more and more high-sulfur gas reservoirs have been discovered in China. The biggest difference between high-sulfur natural gas and conventional natural gas is the presence of hydrogen sulfide gas. During the development of high-sulfur gas, as the gas pressure, temperature, and flow rate change, elemental sulfur will be precipitated in the gas. When the elemental sulfur continues to accumulate and become larger, so that it cannot be carried away by the gas, sulfur deposition will occur. During the operation of surface pipelines, different components and phases of the conveying medium have different degrees of erosion and corrosion on the surface pipeline...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N17/02
CPCG01N17/02
Inventor 曾德智张恩搏喻智明董宝军施太和张智侯铎钟显康张乃艳
Owner SOUTHWEST PETROLEUM UNIV
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