Full-view-field quantitative statistical distribution representation method of precipitated phase particles in metal material

A technology of statistical distribution of metal materials, applied in particle and sedimentation analysis, material analysis through optical means, metal testing, etc., can solve problems such as inhomogeneity and low efficiency of manual image modification, and achieve large field of view and statistical The data is accurate and reliable, eliminating the effect of incomplete statistics

Active Publication Date: 2018-06-29
CENT IRON & STEEL RES INST
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Problems solved by technology

[0005] In view of the above technical problems, the purpose of the present invention is to provide a full-field quantitative statistical distribution characterization method of precipitated phase particles in metal materials, to eliminate the subjective error caused by manual selection of the field of view and to avoid the statistical omission of precipitated phase particles, to solve The problem of inefficiency caused by manual modification of images, while taking into account the characteristics of inhomogeneity of the material itself, provides a more representative, comprehensive, accurate and efficient characterization of the quantitative statistical distribution of precipitated phase particles in a large range of the metal material. detection means

Method used

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  • Full-view-field quantitative statistical distribution representation method of precipitated phase particles in metal material
  • Full-view-field quantitative statistical distribution representation method of precipitated phase particles in metal material
  • Full-view-field quantitative statistical distribution representation method of precipitated phase particles in metal material

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Embodiment

[0086] This example is a nickel-based superalloy for aero-engine turbine disks. This precipitation-hardening nickel-based superalloy is a key heat-resistant material for manufacturing aero-engines, gas turbines, nuclear reaction equipment, etc., and its development level has become an important symbol of a country's aviation industry level. . With the improvement of engine thrust-to-weight ratio and performance requirements, the turbine inlet temperature is constantly increasing, and higher requirements are placed on the temperature of the turbine disk alloy. There are differences, especially the cooling rate will form a gradient distribution on the thickness section, resulting in differences in the number, size and distribution of the γ' phase in different regions, so the γ' of nickel-based superalloys in a large range must be Only by performing quantitative statistical distribution characterization of phases can we obtain a more reliable law of the influence of γ' relative t...

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Abstract

The invention belongs to the technical field of the quantitative statistical distribution analysis of characteristic chromatograms of microstructures and precipitated phases in metal materials, and relates to a full-view-field quantitative statistical distribution representation method of precipitated phase particles in a metal material. The method comprises the following steps of electrolytic corrosion of a metallic material sample, automatic collection of a characteristic chromatogram of a metallurgical structure, automatic splicing and fusion of the characteristic chromatograms of full-view-field metallurgical structures, automatic identification and segmentation of the precipitated phase particles and quantitative distribution representation of the large-range full-view-field precipitated phase particles. According to the full-view-field quantitative statistical distribution representation method, through establishing a mathematic model, the automatic splicing and fusion of the characteristic chromatograms of the full-view-field large-area metallurgical structures in a characteristic region and the automatic segmentation and identification of the precipitated phase particles are realized; the quantitative statistical distribution representation information of the full-view-field morphology, quantity, size, distribution and the like of plentiful precipitated phases in a larger range is quickly obtained, and the method has the features of being accurate and high-efficiency and large in quantitative distribution representation information quantity, and has much more statistical representativeness compared with conventional single-view-field quantitative image analysis.

Description

technical field [0001] The invention belongs to the technical field of quantitative statistical distribution analysis of characteristic maps of microstructures and precipitated phases in metal materials, and relates to a full-field quantitative statistical distribution characterization method of precipitated phase particles in metal materials. Background technique [0002] The phases in the material that are distributed in the matrix in a discontinuous state and cannot be surrounded by other phases are collectively referred to as precipitated phases, which are precipitated in the grain or at the grain boundary and have a different crystal structure or lattice constant from the matrix structure. The new phase has an obvious interface with the matrix structure, so the precipitated phase plays a very important role in the steel, and has a great impact on the strength, toughness, plasticity, deep drawability, fatigue, wear, fracture, corrosion and many important physical and chem...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/84
CPCG01N21/84G01N2015/0061G01N15/1475G01N15/0227C25F3/22G01N1/32G06T7/0004G06T7/11G06T7/187G06T7/155G06T2207/10056G06T2207/20152G06T2207/20041G06T2207/30136G01N33/204G06T3/0068G06T7/174G06T7/70G06T2207/20221G06T2207/10148G01N33/20G06V20/695
Inventor 李冬玲沈学静赵雷王海舟万卫浩韩冰卢毓华冯菲菲李超
Owner CENT IRON & STEEL RES INST
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