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181results about "Testing metal structures" patented technology

Full-view-field quantitative statistical distribution representation method of precipitated phase particles in metal material

The invention belongs to the technical field of the quantitative statistical distribution analysis of characteristic chromatograms of microstructures and precipitated phases in metal materials, and relates to a full-view-field quantitative statistical distribution representation method of precipitated phase particles in a metal material. The method comprises the following steps of electrolytic corrosion of a metallic material sample, automatic collection of a characteristic chromatogram of a metallurgical structure, automatic splicing and fusion of the characteristic chromatograms of full-view-field metallurgical structures, automatic identification and segmentation of the precipitated phase particles and quantitative distribution representation of the large-range full-view-field precipitated phase particles. According to the full-view-field quantitative statistical distribution representation method, through establishing a mathematic model, the automatic splicing and fusion of the characteristic chromatograms of the full-view-field large-area metallurgical structures in a characteristic region and the automatic segmentation and identification of the precipitated phase particles are realized; the quantitative statistical distribution representation information of the full-view-field morphology, quantity, size, distribution and the like of plentiful precipitated phases in a larger range is quickly obtained, and the method has the features of being accurate and high-efficiency and large in quantitative distribution representation information quantity, and has much more statistical representativeness compared with conventional single-view-field quantitative image analysis.
Owner:CENT IRON & STEEL RES INST

Etchant for displaying 690 nickel-base alloy deposited metal grain boundary and etching method thereof

The invention discloses an etchant for displaying a 690 nickel-base alloy deposited metal grain boundary and an etching method thereof. The etchant comprises ferric chloride, EDTA, deionized water andconcentrated hydrochloric acid. The surface of the 690 nickel-based alloy deposited metal surface is successively wiped with the etchant and a nitric acid ethanol solution. Thus, it is possible to intuitively observe that the surface of a sample changes from bright to frosty during an etching process, and the weld bead can be clearly observed by naked eyes in order to better control the degree ofcorrosion, completely and clearly show the grain boundaries of the deposited metal sample grains, and avoid the covering by corrosion products. The etched different grains have different shades due to different orientations. The columnar crystal structure can be clearly observed and the grain boundaries are clear and complete. The etchant is made of simple raw materials, nontoxic, environmentallyfriendly, convenient in liquid waste disposal, low in cost, and stable and easy to control in a reaction process. The etching method is simple and easy to use, and provides detection basis for the process quality control, the process plan and the quality analysis of nuclear welding deposited layer, and has very important practical significance.
Owner:SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING +1

Method for analyzing post-dynamic recrystallization process of high-strength steel

The invention discloses a method for analyzing the post-dynamic recrystallization process of high-strength steel and belongs to the field of plastic forming. The method comprises the following steps that 1, a cylindrical sample is prepared; 2, a single-pass compression experiment is conducted at different deformation temperatures, strain states and deformation, and after the deformation of the sample reaches a preset value, the sample is quenched immediately; 3, the quenched sample is sliced in the axis direction of the sample; 4, slices are subjected to infrared heating to the target temperature in a high-temperature laser confocal in-situ observation experiment and then subjected to heat preservation, real-time in-situ observation is conducted, and metallograph in the metallographic structure changing process is shot; and 5, the grain sizes and dynamic recrystallization volume fractions at different time are obtained through the metallograph, and then the influence of different parameters on the post-dynamic recrystallization process is analyzed. According to the method for analyzing the post-dynamic recrystallization process of the high-strength steel, a thermocompression experiment method and an in-situ observation experiment method are combined, real-time dynamic observation can be achieved, experiment precision is improved, materials are saved, the period is shortened, and the cost is lowered.
Owner:HUAZHONG UNIV OF SCI & TECH

Experiment method for adjusting local sate of titanium alloy Alpha/Beta phase interface

The invention discloses an experiment method for adjusting a local sate of a titanium alloy Alpha/Beta phase interface. The experiment method comprises the steps of processing a titanium alloy experiment sample to form a cylindrical shape, additionally arranging electrodes at two ends of a part of sample, and performing pulse current impact processing, wherein no pulse current impact processing isperformed on the other part of sample; cutting the sample along a middle line, and processing a cutting surface to obtain a sample which can be observing a gold phase; observing morphology of a Alphaphase and a Beta phase and change of the Alpha/Beta phase interface of the titanium alloy which is subjected to pulse current impact processing or is not subjected to pulse current impact processingby a scanning electron microscope under high power, and performing contrast to obtain an evolution rule of the titanium alloy Alpha/Beta phase after pulse current impact processing; and analyzing thestate change of the titanium alloy Alpha/Beta phase after the pulse current impact processing by a pulse current impact thermal effect and non-thermal effect action mechanism so as to obtain experiment conclusion. According to the method, the local state of the titanium alloy Alpha/Beta phase interface is adjusted by pulse current impact, the experiment method is low in time consumption and high in efficiency, and the change effect can be observed and verified.
Owner:WUHAN UNIV OF TECH

Metallographic corrosion method for high-carbon martensitic stainless steel grain boundary

The invention belongs to the field of metallographic analysis and detection of stainless steel, and particularly relates to a metallographic corrosion method for high-carbon martensitic stainless steel grain boundary. The problem that a metallographic corrosion method which aims at high-carbon martensitic stainless steel, is easy and convenient to operate and low in cost is lacked is solved. The invention provides the metallographic corrosion method of a high-carbon martensitic stainless steel grain boundary, wherein the method comprises the following steps: carrying out coarse grinding, finegrinding, polishing, cleaning and drying on a high-carbon martensitic stainless steel metallographic sample to obtain a bright scratch-free polished surface; and corroding the polished surface for 5-30 s at room temperature by adopting a metallographic corrosive agent, cleaning and drying. The metallographic corrosive agent is composed of 1 g to 4 g of picric acid, 5 ml of concentrated hydrochloric acid, 100 ml of ethyl alcohol and 2 ml to 5 ml of dishwashing liquid. The method aims at the high-carbon martensitic stainless steel, the grain boundary display effect is good, normal-temperature corrosion is adopted without pre-heating the sample, the corrosion time is short, operation is easy, and application and popularization are easy.
Owner:什邡新工金属材料有限公司

Hardware crimping quality probing device capable of carrying out nondestructive testing

InactiveCN111272967AQuick fixFast and uniform detectionTesting metal structuresElectric machineryEngineering
The invention discloses a hardware fitting crimping quality probing device capable of carrying out nondestructive testing. The device comprises a mounting plate and a detector, the upper end of the mounting plate is fixedly connected with a portal frame; the opposite sides of the two vertical parts of the portal frame are connected with the detector through a moving mechanism. The side wall of onevertical part of the portal frame is slidably sleeved with a rectangular rod through a rectangular through hole; one end of the rectangular rod penetrates through the rectangular through hole and isrotationally connected with a fixed plate through a first rolling bearing; a T-shaped sliding groove is formed in the rod wall of the rectangular rod, a limiting mechanism is arranged in the T-shapedsliding groove, a motor is fixedly connected to the side wall of the other vertical part of the portal frame, a rotating shaft is fixedly connected to the output end of the motor, and one end of the rotating shaft penetrates through the side wall of the vertical part of the portal frame and is fixedly connected with a rectangular block. According to the invention, workers can conveniently and rapidly fix hardware fittings, the surfaces of the hardware fittings can be rapidly and uniformly detected, and meanwhile, the hardware fittings with different lengths can be detected.
Owner:马鞍山市华能电力线路器材有限责任公司

Metallographic corrosion method for simultaneously displaying austenitic stainless steel and aluminide coating organization structure on surface of austenitic stainless steel

ActiveCN111982645ASimultaneous imaging effect is remarkableCorrosion method is simple and effectiveMaterial analysis using wave/particle radiationNuclear energy generationSS - Stainless steelCopper sulfate
The invention provides a metallographic corrosion method for simultaneously displaying austenitic stainless steel and an aluminide coating tissue structure on the surface of the austenitic stainless steel. The method comprises the following steps: mixing 40-55% of hydrochloric acid, 37-48% of ultrapure water and 8-12% of glycerol in percentage by volume to obtain a liquid phase, and then adding copper sulfate and ferric trichloride to obtain a metallographic corrosive agent; uniformly dripping the prepared metallographic corrosive agent on the surface of the coating sample to corrode for 15-25seconds; after the surface gradually loses the finish degree, immediately using a large amount of ultrapure water for washing, finally, sucking absolute ethyl alcohol or acetone to clean residual water spots and impurities on the surface of the sample, using a blower used for blow-drying so that the austenite steel and the organization structure of the aluminide coating on the surface of the austenite steel can be developed at the same time. The corrosion method is mainly used for simultaneously developing organizational structures of the austenitic stainless steel and the aluminide coating on the surface of the austenitic stainless steel, and has a remarkable effect of simultaneously developing a matrix and a coating structure in an original state and a service state.
Owner:XIAN THERMAL POWER RES INST CO LTD

Martensite aging stainless steel dendritic crystal corrodent and corrosion method

The invention relates to a martensite aging stainless steel dendritic crystal corrodent and corrosion method, and belongs to the technical field of metallographic analysis of iron and steel. The corrodent provided by the invention is an analytical pure nitric acid aqueous solution, which is prepared from an analytical pure nitric acid and water. The dendritic crystal corrosion method comprises thesteps of: a. cutting an as-cast sample for grinding and polishing; b. preparing the dendritic crystal corrodent; and c. using a stainless steel sheet as a cathode, using the sample as an anode, and placing the as-cast sample in the corrodent to perform electrolytic etching at room temperature. The corrodent provided by the invention has a simple formula, simple operation steps, and clear and accurate detection results of dendritic crystal corrosion, data such as interdendritic spacing can be accurately calculated through clear morphology of the dendritic crystal, and segregation degrees between dendritic crystals and dendritic crystal stems can be measured by using an energy spectrum for evaluating quality of the as-cast structures and assisting in evaluating the elimination of dendriticsegregation by the homogenization heat treatment.
Owner:CHENGDU ADVANCED METAL MATERIALS IND TECH RES INST CO LTD

Method for preparing high-melting-point metal ternary diffusion couple

The invention discloses a method for preparing a high-melting-point metal ternary diffusion couple. The method is mainly used for preparing the diffusion couple composed of three kinds of high-melting-point metal. The method comprises the following steps: paving a B metal block or sheet with the lowest melting point in three kinds of high-melting-point metal above an A metal block, then putting A-B metal into a tubular furnace protected by argon, heating to be above the melting point of the B metal, melting the B metal to form metallurgical bonding with the A, and performing diffusion annealing to form an A-B diffusion couple; and then coating the C metal sheet at the interface of the A-B diffusion couple, fixing the C metal sheet by using a clamp, and performing diffusion annealing to prepare the A-B/C ternary diffusion couple. The method is simple, the amount of needed metal is small, the preparation process is easy to control, diffusion couple combination is flexible and controllable, the effect is excellent, and the success rate is high. The method is suitable for preparation of metal material diffusion couples, especially for preparation of precious metal and high-temperature alloy material diffusion couples, and the prepared diffusion couples can be used for research of phase diagrams, diffusion kinetics and thermodynamics.
Owner:KUNMING INST OF PRECIOUS METALS

Component-based special steel performance evaluation method and system

The invention provides a component-based special steel performance evaluation method and system, and relates to the technical field of artificial intelligence, and the method comprises the steps: carrying out the component detection of a first special steel material, and obtaining first component information and first proportion information; performing structural analysis on the first special steel material to obtain first crystal information; performing performance analysis on the first application scene to obtain first performance deviation sorting information; performing performance evaluation on the first special steel material according to the first component information and the first proportion information to obtain a first performance evaluation result; adjusting the first performance evaluation result according to the first crystal information to obtain a second performance evaluation result; and when the first performance deviation sorting information is not met, the first component information, the first proportion information and the first crystal information are optimized, so that the technical problem that the combination degree of special steel preparation process parameters and application scenes is difficult to guarantee due to judgment depending on personnel experience is solved. And the technical effect of obtaining the special steel process parameters with high combination degree with the application scene is achieved.
Owner:SUZHOU XIANGLOU METAL PROD

Method for analyzing microstructure nucleation mechanism of laser welding seam

The invention belongs to the technical field related to laser welding, and discloses a method for analyzing a microstructure nucleation mechanism of a laser welding seam. The method comprises the following steps: (1) performing laser welding, namely test welding, on a sample 1, and analyzing the microstructure morphology and distribution of the obtained laser welding seam; meanwhile, using TIG welding for conducting one-pass pre-welding and n-pass pre-welding on the sample 2-1 and the sample 2-2 correspondingly, then conducting test welding on weld joints formed through pre-welding correspondingly, and conducting metallographic representation on the obtained overlapped weld joints correspondingly; wherein the sample 1, the sample 2-1 and the sample 2-2 are made of the same material; wherein n is a positive integer greater than or equal to 3; (2) comparing the equiaxed crystal quantity and distribution of the laser weld joint and the overlapped weld joint area of the sample 1, and pre-identifying the nucleation mechanism of the weld joint according to the comparison result; and (3) performing confirmation according to the pre-identification result so as to analyze and obtain a nucleation mechanism. According to the invention, the accuracy and repeatability of a nucleation mechanism are improved.
Owner:HUAZHONG UNIV OF SCI & TECH

Production and processing equipment with automobile shifting fork welding assembly detection function

The invention discloses production and processing equipment with an automobile shifting fork welding assembly detection function. The production and processing equipment comprises a shifting fork feeding case, and a shifting fork feeding bin is fixedly welded on the right side of the upper surface of the top of the shifting fork feeding case; an arc-shaped sliding groove is fixedly welded on the right side of the surface of a control console; a motor controller is arranged at the bottom of a small arm of a rotary mechanical arm, and a second conveyor belt is arranged on the surface of the right side of the rotary mechanical arm; and a discharging port is formed in the bottom of the front side of the rotary mechanical arm. According to the production and processing equipment, the control console is arranged between the shifting fork feeding case and the rotary mechanical arm; single-column pneumatic cylinders are arranged at the bottoms of the shifting fork feeding case and the rotary mechanical arm separately, thereby facilitating pushing of a driven sliding block to enable a control console to rise upwards; meanwhile, through arrangement of the arc-shaped sliding groove, a weldinghead is easy to move along the arc-shaped sliding groove, and the problem of low precision during manual welding is solved; and thus, automatic welding is facilitated, and the welding precision is improved.
Owner:东莞市夯实科技有限公司
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