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214results about "Investigating crystals" patented technology

Method for displaying original austenite grain boundary of 85Cr2MnMo liner steel

The invention discloses a method for displaying the original austenite grain boundary of 85Cr2MnMo liner steel. The method comprises the following steps: (1) sample preparation; (2) determination of phase transition temperature, wherein Accm (complete dissolution of cementite and carbide into austenite) temperature of the 85Cr2MnMo liner steel is 835 DEG C according to results of thermal expansion measurement; (3) quenching: heating a sample to 860 to 920 DEG C, maintaining the temperature for 60 min and then rapidly quenching the sample in machine oil No. 10; and (4) corrosion: mixing 100 ml of deionized water, 4 g of picric acid, 2 g of Aiou shampoo paste and 0.1 g of CuCl2.2H2O to prepare a corrosive agent, putting the corrosive agent in a water-bath pot with a temperature of 55 to 60 DEG C for heat preservation, putting the quenched, ground and polished sample in the corrosive agent for corrosion for 50 to 60 s, taking the sample out, wiping the sample with absorbent cotton dipped with alcohol so as to remove reaction products on the surface of the sample, cleaning the sample through flushing and then subjecting the sample to blow-drying. As the sample is observed with an optical microscope, the original austenite grain boundary of 85Cr2MnMo liner steel can be clearly displayed and matrix structure is not displayed, so bases are provided for accurate rating of the grain size of austenite.
Owner:SHANGHAI UNIV

Photo-thermal common-path interference module and method for measuring crystal defect

The invention discloses a photo-thermal common-path interference module which is applied to a crystal defect measurement instrument. The crystal defect measurement instrument based on a module is characterized in that pump laser and detection laser are focused at the same point of a sample to test a dynamical mesoscopic defect of the sample; a dynamic defect three-dimensional distribution map of the sample is obtained through movement of the sample. The photo-thermal common-path interference module disclosed by the invention comprises a pumping light source, a detection light source, a converging light path, a sample frame, a measurement light path, a laser power meter, and a wave-front detector, wherein a test point is heated through the pump laser; remaining laser is received by the laser power meter; the detection laser passes through the heated test point; interference is changed in front of waves according to the temperature distribution of the test point; weak laser passing through the sample passes through the measurement light path, and is irradiated into the wave-front detector; changed wave-front information is measured, and the heating condition and absorption capacity of an irradiation point are obtained through comparative calculation.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Ultrahigh-flux platform for screening crystal generation conditions and screening method

The invention discloses an ultrahigh-flux platform for screening crystal generation conditions and a screening method. The platform comprises a micro-fluidic droplet chip, a micro-droplet collection chip and a characterization-analysis system, wherein the micro-fluidic droplet chip is used for generating crystallized droplets at ultrahigh flux; the micro-droplet collection chip is used for collecting the crystallized droplets generated by the micro-fluidic droplet chip; and after the micro-droplet collection chip collects the crystallized droplets, the characterization-analysis system characterizes and identifies the morphology of crystals in the crystallized droplets, and analyzes and screens out crystallization conditions corresponding to the optimal crystal morphology according to the characterized and identified morphology of the crystals. The ultrahigh-flux platform provided by the invention provides a good solution for rapid screening of crystal generation conditions. The screening method for screening the crystal generation conditions provided by the invention is based on the ultrahigh-flux platform, can quickly screen out excellent and stable crystallization conditions, andis convenient and accurate.
Owner:SUN YAT SEN UNIV

Visualization device and method for multidirectional observation of hydrate generation and decomposition

ActiveCN107064145AAvoid high pressure and low temperature conditionsSolve the problem of water mistInvestigating crystalsTemperature controlAcquisition apparatus
The invention relates to a visualization device and method for multidirectional observation of hydrate generation and decomposition. The visualization device comprises a low-temperature constant-temperature control system, a normal-pressure visualization reaction device, a temperature acquisition apparatus and a CCD imaging system, wherein the normal-pressure visualization reaction device comprises a temperature control circulating tank, a reaction tank, a circulating liquid inlet and a circulating liquid outlet; the reaction tank is arranged in the temperature control circulating tank; the tank wall of the temperature control circulating tank is communicated with the circulating liquid inlet and the circulating liquid outlet; a two-layer organic glass window is arranged on one side tank wall of the reaction tank, and comprises an observation window and an organic glass window in turn from inside to outside; the observation window and the organic glass window are both made of organic glass. According to the visualization device and method provided by the invention, the two-layer organic glass window is adopted, and is totally closed inside, air is dry, and the heat conductivity is low; the temperature of the outer-layer organic glass is close to room temperature, and the problem of water mist is solved.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Prediction method and device for continuous casting center segregation

The invention provides a prediction method and device for continuous casting center segregation. The method comprise: obtaining continuous casting billet image information, and inputting the continuous casting billet image information into a training model, wherein the training model is obtained by training multiple sets of training data, and each set of training data comprises the continuous casting billet image information and a label for recognizing billet process information on the continuous casting billet image information; obtaining output information of the training model, wherein theoutput information comprises billet process information corresponding to the continuous casting billet image information; and according to the billet process information corresponding to the continuous casting billet image information and the standard continuous casting billet process threshold, obtaining billet prediction information, and predicting whether the billet corresponding to the continuous casting billet image is subjected to center segregation. The technical problems that in the prior art, a casual inspection mode is adopted, judgment cannot be conducted one by one, and center segregation of continuous casting billets cannot be predicted in advance are solved. The technical effects that intelligent data processing is conducted on all steel billets in the continuous casting equipment, the risk of center segregation is predicted in time, the accuracy is high, and the quality of the steel billets is improved are achieved.
Owner:LIANFENG STEEL (ZHANGJIAGANG) CO LTD

Etchant for displaying 690 nickel-base alloy deposited metal grain boundary and etching method thereof

The invention discloses an etchant for displaying a 690 nickel-base alloy deposited metal grain boundary and an etching method thereof. The etchant comprises ferric chloride, EDTA, deionized water andconcentrated hydrochloric acid. The surface of the 690 nickel-based alloy deposited metal surface is successively wiped with the etchant and a nitric acid ethanol solution. Thus, it is possible to intuitively observe that the surface of a sample changes from bright to frosty during an etching process, and the weld bead can be clearly observed by naked eyes in order to better control the degree ofcorrosion, completely and clearly show the grain boundaries of the deposited metal sample grains, and avoid the covering by corrosion products. The etched different grains have different shades due to different orientations. The columnar crystal structure can be clearly observed and the grain boundaries are clear and complete. The etchant is made of simple raw materials, nontoxic, environmentallyfriendly, convenient in liquid waste disposal, low in cost, and stable and easy to control in a reaction process. The etching method is simple and easy to use, and provides detection basis for the process quality control, the process plan and the quality analysis of nuclear welding deposited layer, and has very important practical significance.
Owner:SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING +1
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