Device and method for increasing concentration of volatile sample and matter detector

A technology of volatile substances and sample concentration, which is applied in the field of mass spectrometry, can solve the problems of complicated and time-consuming processing of volatile organic substances, and achieve the effects of low cost, high gas concentration and high concentration

Active Publication Date: 2018-11-13
SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

For example, when sampling and testing volatile organic compounds in waste liquid from chemical plants, distillation and other steps are required to gasify them and then use analytical instruments to detect their gas substances; sampling and testing of volatile organic compounds in soil requires collection by methods such as purge and trapping The volatile organic compound treatment process is complicated and time-consuming

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  • Device and method for increasing concentration of volatile sample and matter detector

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Embodiment Construction

[0020] Embodiments of the present invention will be described in detail below. It should be emphasized that the following description is only exemplary and not intended to limit the scope of the invention and its application.

[0021] refer to figure 1 , in one embodiment, a device for increasing the concentration of volatile samples, including a sample container 1, a piston 3 arranged in the sample container 1, a storage chamber 7, and a storage chamber 7 arranged in the The piston 6, the gas pipeline 4 connected to the sample container 1, the gas pipeline 9 connected to the storage chamber 7, the sample container 1 is sealed by the piston 3, and passes through the gas pipeline 4 It is connected to the storage cavity 7, which is sealed by the piston 6, and connected to the detection instrument (not shown in the figure) through the gas pipeline 9. When the piston 3 slides from the initial position along the first direction ( figure 1 middle is sliding upward), the volume in...

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Abstract

The invention discloses a device and method for increasing the concentration of a volatile sample. The device comprises a sample container and a storage cavity, wherein the sample container is sealedby a piston and connected to the storage cavity by a first gas circuit pipeline, the storage cavity is sealed by a piston and is connected to a detecting instrument by a second gas circuit pipeline, and when the piston in the sample container slides from an initial position along a first direction, the volume in the sample container increases, and the air pressure decreases, so that a volatile matter in a sample in the sample container volatilizes more intensely, and the gas concentration increases; the volatile matter is transported from the sample container into the storage chamber through the first gas circuit pipeline, and then is pressurized and compressed by the piston to increase the sample concentration; valves of the first gas circuit pipeline and the second gas circuit pipeline are controlled to open and close to control the volatile matter of the sample to be continuously or discontinuously delivered to the detecting instrument. The device can increase the gas concentrationof the volatile matter in the sample in a simple and effective manner without complicated pretreatment, and has a simple structure and high efficiency.

Description

technical field [0001] The invention relates to the field of mass spectrometry analysis, in particular to a device, method and substance detection device for increasing the concentration of volatile samples. Background technique [0002] Mass spectrometry is a fast and efficient material detection and analysis method, which is widely used in food and drug safety, space science exploration, public safety and other fields. Volatile organic compounds such as toluene, anisole, xylene, etc. are often dissolved in liquids or absorbed by solids. For example, when sampling and testing volatile organic compounds in waste liquid from chemical plants, distillation and other steps are required to gasify them and then use analytical instruments to detect their gas substances; sampling and testing of volatile organic compounds in soil requires collection by methods such as purge and trapping The VOC treatment process is complicated and time-consuming. Contents of the invention [0003...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/40G01N27/62
CPCG01N1/40G01N27/62
Inventor 余泉张乾王晓浩
Owner SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV
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