Walnut shell biomass c/fe 3 o 4 Preparation method of /cu microwave absorbing material
A microwave-absorbing material and biomass technology, applied in chemical instruments and methods, and other chemical processes, can solve problems such as low comprehensive utilization rate and complex structure, and achieve good microwave-absorbing performance, reasonable design, and good promotion and application value Effect
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[0021] Specific embodiments of the present invention will be described in detail below.
[0022] A kind of walnut shell biomass C / Fe 3 o 4 The preparation method of / Cu microwave absorbing material comprises the steps:
[0023] (1) The walnut shells are dried, crushed, and sieved to particles below 500 μm for later use.
[0024] (2), 2.59g FeCl 3 ·6H 2 O was dissolved in 200mL aqueous solution, fully stirred and dissolved to form a solution for later use.
[0025] (3) Add 1~10g of the walnut shell powder prepared in step (1) to the ferric chloride solution in step (2), stir and soak fully for about 0.5h, filter and dry to obtain walnut shell powder / FeCl 3 solid.
[0026] (4), 2.27g FeCl 2 4H 2 Add O and 0.5g copper powder to 100mL ethanol, add 0.05~0.5g sodium lauryl sulfate, carry out ultrasonic dispersion for 0.5~2h, after the dispersion is completed, add step (3) walnut shell powder / FeCl 3 Solid, fully stirred and soaked for about 0.5h, filtered and dried to obtain ...
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