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820 results about "Carbonyl iron" patented technology

Carbonyl iron is a highly pure (97.5% for grade S, 99.5+% for grade R) iron, prepared by chemical decomposition of purified iron pentacarbonyl. It usually has the appearance of grey powder, composed of spherical microparticles. Most of the impurities are carbon, oxygen, and nitrogen.

Broadband wave-absorbing material and preparation method thereof

ActiveCN106380626AAchieve broadband absorbing performanceStrong designabilitySurface layerBroadband
The invention discloses a broadband wave-absorbing material and a preparation method thereof. The broadband wave-absorbing material is composed of a low frequency wave-absorbing material bottom layer and a high frequency wave-absorbing material surface layer. The high frequency wave-absorbing material surface layer comprises a plurality of high frequency wave-absorbing layers with different concentrations. FeSi or FeSiAl particles are taken as the additive of the low frequency wave-absorbing material, and carbonyl iron particles are taken as the additive of the high frequency wave-absorbing material. A rolling method is adopted to prepare the low frequency wave-absorbing material bottom layer, and a three-dimensional moulding technology is adopted to prepare the high frequency wave-absorbing material surface layer. The multilayer lamination manufacturing method combines a multi-rolling technology and three-dimensional moulding together and has the advantages that the binding force between layers can be ensured, multiple repeated mould pressing is avoided, the thickness of each layer, the internal structure, and particle distribution can be adjusted so as to satisfy the predetermined electromagnetic property requirements; the broadband wave-absorbing performance of the wave-absorbing material and designable performance of a shielding material can be realized; the integrated manufacturing of space structure of the wave-absorbing material is achieved, and the preparation cost is low at the same time.
Owner:SHANGHAI RADIO EQUIP RES INST

Water-based magneto-rheological polishing liquid for optical processing and preparation method thereof

The invention relates to a water-based magnetorheological polishing solution for optical manufacture, which is formed by the following volume components, water-based remixed carrier liquid 25%-75% and additive component 25%-75%, wherein the additive component is dispensed by the following volume percentage, carbonyl iron powder 80%-90%, nanometer iron powder 4%-10% and polishing powder 4%-10%, the water-based remixed carrier liquid which is measured according to volume percentage comprises deionized water 85%-90%, dispersing agent 3%-5%, wetting agent 2%-5% and thixotropic agent 3%-5%, the method for preparing comprises the following steps: mixing deionized water and thixotropic agent, stirring in indoor temperature for 1-2 hours, and adding dispersing agent, stirring in indoor temperature for 0.5-1 hour, and then adding wetting agent, stirring in indoor temperature for 0.5-1 hour, getting water-based remixed carrier liquid, mixing additive component and water-based remixed carrier liquid, adding into a ball-milling tank, adding into a steel ball according to mass ratio which is 1:10, grinding for 3-5 hours in the speed which is 20-30r/m, separating out a steel ball, and getting products. The polishing solution of the invention has the advantages of excellent stability, high rheological property, excellent oxidation resistance property and simple and environmental-friendly preparation technology.
Owner:NAT UNIV OF DEFENSE TECH

Magnetic nanoparticle-based immobilized laccase and ionic liquid composite particle and application thereof

The invention discloses a magnetic nanoparticle-based immobilized laccase and an ionic liquid composite particle, a preparation method thereof and application in removal of contaminants in water. The preparation method comprises the steps that carbonyl iron is taken as an iron source and is synthesized to be gamma-Fe2O3 nano-particles through a chemical precipitation method; the magnetic nanoparticles are taken as cores, tetraethoxysilane and a silane coupling agent are taken as a silicon source, and by means of a sol-gel method, surface amino-functionalized nano core-shell type magnetic silicon dioxide is prepared; 1-ethyl-(3-dimethyllaminopropyl) carbodiie hydrochlide is taken as a coupling agent, and laccase is bonded on the surface of the nano core-shell type magnetic silicon dioxide in a covalent bond manner to obtain the immobilized laccase of the magnetic nanoparticle silicon dioxide particles; and then the immobilized laccase is reacted with a functionalized ionic liquid which is synthesized by reacting N,N-carbonyldiimidazole and an ionic carboxy contained liquid to prepare the magnetic nanoparticle immobilized laccase and ionic liquid composite particle, and the composite particle is applied to the removal of the contaminants in water.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method for flaky carbonyl iron powder with high magnetic permeability

The invention relates to a preparation method for flaky carbonyl iron powder with high magnetic permeability, and belongs to the field of magnetic wave absorbing materials. The method comprises the following steps: 1, carrying out a primary ball milling process: at a room temperature, weighing 100-150 g of steel balls with a diameter of 3-6 mm, 5-10 g of carbonyl iron powder, and 0.01-0.1 g of a surfactant calcium stearate, measuring 30-50 ml of an organic solution, adding the materials and the solution to a 100 ml ball mill tank, and carrying out ball milling in a planetary type ball mill; 2, washing the carbonyl iron powder with the primary ball milling three times by using ethanol, and carrying out blow-drying at a room temperature or carrying out rapid drying at a temperature of 50-70 DEG C; 3, carrying out a secondary ball milling process: mixing the dried carbonyl iron powder and steel balls with a diameter of 3-6 mm according to the ratio of the primary ball milling process described in the step 1, and then carrying out ball milling for 2-10 minutes at a speed of 400-600 rotation/min; and 4, cooling the ball milling tank, and then separating the iron powder and the steel balls to obtain the flaky carbonyl iron powder sample. The process of the preparation method of the present invention is simple. With the preparation method of the present invention, a dielectric property is not changed while high magnetic permeability is provided.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Methods of improving surface roughness of an environmental barrier coating and components comprising environmental barrier coatings having improved surface roughness

Methods for improving surface roughness of an environmental barrier coating including providing a component having a plasma sprayed environmental barrier coating; applying a slurry to the environmental barrier coating of the component, the slurry being a transition layer slurry or an outer layer slurry; drying the environmental barrier coating having the applied slurry; and sintering the component to produce a component having an improved surface roughness where the slurry includes a solvent; a primary transition material, or a primary outer material; and a slurry sintering aid selected from iron oxide, gallium oxide, aluminum oxide, nickel oxide, titanium oxide, boron oxide, alkaline earth oxides, carbonyl iron, iron metal, aluminum metal, boron, nickel metal, iron hydroxide, gallium hydroxide, aluminum hydroxide, nickel hydroxide, titanium hydroxide, alkaline earth hydroxides, iron carbonate, gallium carbonate, aluminum carbonate, nickel carbonate, boron carbonate, alkaline earth carbonates, iron oxalate, gallium oxalate, aluminum oxalate, nickel oxalate, titanium oxalate, solvent soluble iron salts, solvent soluble gallium salts, solvent soluble aluminum salts, solvent soluble nickel salts, solvent titanium salts, solvent soluble boron salts, and solvent soluble alkaline earth salts.
Owner:GENERAL ELECTRIC CO

Irradiation crosslinking low-smoke halogen-free flame-retardant polyolefin cable material for photovoltaic cables

The invention provides an irradiation crosslinking low-smoke halogen-free flame-retardant polyolefin cable material for photovoltaic cables. The cable material is prepared from the following raw materials in parts by weight: 40-50 parts of polyethylene (PE), 30-40 parts of polyvinyl chloride resin, 20-30 parts of CSM2305, 10-12 parts of ethylene-acrylate copolymer, 10-15 parts of epichlorohydrin rubber T3100, 5-10 parts of epoxidized soybean oil, 2-3 parts of carbonyl iron powder, 10-12 parts of high abrasion carbon black N330, 5-10 parts of light calcium carbonate, 1-2 parts of zinc oxide, 5-10 parts of wollastonite powder, 4-5 parts of vermiculite, 1-2 parts of polytetrafluoroethylene micro powder, 1-2 parts of graphite, 1-2 parts of nano boron carbide, 2-3 parts of ferric oxide, 0.1-0.2 part of UV-O, 0.1-0.2 part of UV-53, 0.1-0.2 part of flame retardant TBC, 10-12 parts of aluminium hypophosphite, 5-8 parts of decabromodiphenyl ether, 8-10 parts of dioctyl terephthalate, 6-8 parts of trioctyl trimellitate, 8-10 parts of triethyl citrate, 1-2 parts of calcium stearate, 0.2-0.4 part of stearic acid, 0.1-0.2 part of oxidized polyethlene wax, 0.2-0.3 part of ethylene bis stearamide, 0.1-0.2 part of DCP, and 12-15 parts of modified filler. The cable material has the characteristics of high flame retardance, high ultraviolet resistance and high ageing resistance, and meanwhile, has a good mechanical property, and is environment-friendly.
Owner:温州市粤来电子加速器应用有限公司

Polyaryl ether nitrile (PEN) and carbonyl iron powder (Fe(CO)5) composite magnetic material and preparation method thereof

The invention discloses a PEN and Fe(CO)5 composite magnetic material and a preparation method thereof, and belongs to the technical field of magnetic polymer materials. PEN serves as an organic matrix, Fe(CO)5 serves as an inorganic filler, and the composite magnetic material is obtained after blending and prilling. Firstly, the Fe(CO)5 is subjected to surface modification, and a layer of phthalonitrile prepolymer is generated on the surface of the Fe(CO)5; due to a layer of organic matters rich in cyan coated on the surface, the Fe(CO)5 after surface modification can improve the interfacial adhesive force between the Fe(CO)5 inorganic filler and the PEN organic matrix, so that the PEN and the Fe(CO)5 are provided with a high-strength magnetic property while maintain an excellent mechanical property of the PEN after composition. According to the magnetic material and the preparation method thereof, the Fe(CO)5 can be filled as much as possible on the premise that the good mechanical property of the composite material is maintained, so that magnetic saturation strength of the composite material can be improved, the compatibility of inorganic fillers with polymers is improved, and processing defects are overcome.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

China Mobile 4G full band absorbing material, and preparation method and application thereof

The invention discloses a China Mobile 4G full band absorbing material, and a preparation method and application thereof. A composite auxiliary agent of a silane coupling agent and a stearate surfactant is added to a carbonyl iron powder, and a high-energy ball milling process is carried out to prepare a sheet-shape carbonyl iron powder absorbing material with excellent impedance matching performance. The material can meet the following requirements: in the frequency range from 1 to 18 GHz, an absorbing coating has thickness of less than or equal to 2mm; the absorbing material has -8dB absorption bandwidth reaching 1.5GHz (1.3-2.8GHz), which completely covers the whole band of China Mobile 4G (1.8GHz-2.8GHz); the proportion of the silane coupling agent and stearate can be adjusted to obtain proper sheet structure and size, thus changing the relationship between the complex permittivity and complex permeability to reach impedance matching, and then adjusting the absorption peak position. The material achieves the purpose of selecting absorption interference noise at three arbitrary main frequencies of China Mobile 4G and improving the signal-to-noise ratio of the base station and mobile terminal.
Owner:南京威勒信息技术科技有限公司

Low viscosity stability non-water-base magnetic rheology polishing liquid and preparation method thereof

The invention discloses non-aqueous magnetorheological polishing fluid which is steady at low viscosity and a preparation method thereof. The non-aqueous magnetorheological polishing fluid comprises basic carrier fluid which accounts for 40 to 75 percent of the total volume of the magnetorheological polishing fluid, 15 to 50 percent of carbonyl iron powder, 3 to 8 percent of surfactant and 3 to 6 percent of polishing powder, wherein, the basic carrier fluid is dimethicone. The preparation method of the invention is as follows: the surfactant is completely dissolved in the basic carrier fluid by heating and stirring, then the magnetic granular carbonyl iron powder and the basic carrier fluid mixture are mixed, then a ball-grinding device of a ball grinder is adopted to disperse the mixture so as to improve the anti-sedimentation property and the stability of the magnetorheological polishing fluid to finally ensure that the prepared magnetorheological polishing fluid always keeps rolling to maintain the stability of the characteristic of the magnetorheological polishing fluid. The polishing fluid prepared by the invention has low zero magnetic field viscosity, big shear yield stress and good magnetorheological performance, is suitable for the processing of deliquescent optical materials, and has a simple preparation process, no toxicity, and low cost.
Owner:NAT UNIV OF DEFENSE TECH

Preparation method of high performance metal magnetic powder core for high frequency nonpolar lamp circuit

ActiveCN101127269AMagnetic permeability range adjustableHigh magnetic permeability and high stabilityInductances/transformers/magnets manufactureElectric discharge lampsOxygenOperating frequency
The utility model discloses a preparation method for a high performance magnetic powder core used for high frequency electrodeless lamp circuits, which is characterized in that first, the carbonyl iron dust with 0.4 to 0.5% carbon, 0.4 to 0.6% oxygen and 0.5 to 0.6% nitrogen, as well as a mean particle size of 1 to 8 micron, is dehumidified; second, the carbonyl iron dust is phosphatized by wet method; third, the carbonyl iron dust is compounded and covered by high temperature resistant silicone and is dried under vacuum and room temperature conditions to get finished carbonyl iron magnetic powder core; fourth, the carbonyl iron magnetic powder core is put into the mold and is processed by dry pressing, thus the high performance magnetic powder core used for high frequency electrodeless lamp circuit is acquired. The utility model has the advantages of adjustable range of magnetic permeability (Me:3 to 35), excellent factor of quality (Q value) under the circumstances that the working frequency is in the range of 100KHz to 100MHz, high stability of high direct current deflector field and low temperature rise magnetic permeability, and therefore is applicable to high frequency electrodeless lamps with the working frequency 2.65MHz.
Owner:JIANGXI YUEAN SUPERFINE METAL
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