Low viscosity stability non-water-base magnetic rheology polishing liquid and preparation method thereof

A technology of magnetorheological polishing and preparation method, which is applied in the direction of polishing compositions containing abrasives, magnetic liquids, polishing compositions, etc., which can solve problems such as easy sedimentation, low viscosity, and easy agglomeration, and achieve shear yield stress Large size, simple preparation process, and low viscosity in zero magnetic field

Inactive Publication Date: 2008-09-10
NAT UNIV OF DEFENSE TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the current magnetorheological polishing process, most of them use water-based magnetorheological polishing fluid. The base carrier fluid of this type of polishing fluid is water, so it is relatively easy to prepare low-viscosity, non-toxic, etc. suitable for magnetorheological polishing. characteristics, but the water-based magnetorheological polishing fluid is recognized as a difficult problem to solve: easy to settle, easy to oxidize, and easy to agglomerate; in addition, because it contains water, its processing range is limited, and it is not suitable for processing optical materials with deliquescent characteristics. Such as potassium dihydrogen phosphate functional crystal
At present, magnetorheological fluids whose base carrier fluid is silicone oil are widely used in magnetorheological dampers, magnetorheological shock absorbers, and magnetorheological sealing devices. The main performance requirements of

Method used

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  • Low viscosity stability non-water-base magnetic rheology polishing liquid and preparation method thereof
  • Low viscosity stability non-water-base magnetic rheology polishing liquid and preparation method thereof
  • Low viscosity stability non-water-base magnetic rheology polishing liquid and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Prepare a non-water-based magnetorheological polishing solution, the polishing powder is cerium oxide, and the preparation steps are as follows:

[0032] Step 1, measure each component according to the polishing liquid formula, wherein, the volume of base carrier liquid dimethyl silicone oil (viscosity is 20CS) is 720ml, carbonyl iron powder (average particle diameter is 4um, iron-containing purity is 98%, relatively The quality factor is 1.9, the effective magnetic permeability is 4), the volume is 200ml, the surfactant mixture stearic acid is 20ml, Span-40 is 10ml, Tween-60 is 6ml, cerium oxide polishing powder with a particle size of 0.5um It is 44ml.

[0033] Step 2. Put the carrier liquid simethicone in a container and heat it evenly to 70°C.

[0034] Step 3. Slowly pour the surfactant mixture prepared in the above ratio into the base carrier liquid container heated in step 2, and stir fully with a stirring rod to completely dissolve the surfactant mixture in the ...

Embodiment 2

[0041] Prepare a non-water-based magnetorheological polishing solution, the polishing powder is aluminum oxide, and the preparation steps are as follows:

[0042] Step 1. Measure each component according to the polishing liquid formula, wherein the base carrier liquid is a mixture of simethicone oil (viscosity 5CS) and simethicone oil (viscosity 10CS), and its volume ratio is 1:1. Total volume is 600ml, and the volume of carbonyl iron powder (average particle diameter is 4um, and iron-containing purity is 98%, and relative quality factor is 1.9, and effective magnetic permeability is 4) is 300ml, and surfactant mixture stearic acid is 30ml, Span-40 is 15ml, Tween-60 is 7ml, and alumina polishing powder with a particle size of 1um is 48ml.

[0043] Step 2. Put the carrier liquid simethicone in a container and heat it evenly to 70°C.

[0044] Step 3, slowly pour the surfactant mixture prepared in the above ratio into the base carrier liquid container heated in step 2, stir full...

Embodiment 3

[0051] Prepare a non-water-based magnetorheological polishing solution, the polishing powder is diamond powder, and the preparation steps are as follows:

[0052] Step 1. Measure each component according to the polishing liquid formula, wherein the base carrier liquid dimethyl silicone oil (viscosity 5CS) is 500ml, carbonyl iron powder (average particle diameter is 4um, the purity of iron content is 98%, and the relative quality factor is 1.9 , effective magnetic permeability is 4) volume is 400ml, surfactant mixture stearic acid is 35ml, Span-40 is 14ml, Tween-60 is 8ml, and the diamond micropowder polishing powder of 1um particle diameter is 43ml.

[0053] Step 2. Put the carrier liquid simethicone in a container and heat it evenly to 70°C.

[0054] Step 3, pour the surfactant mixture prepared in the above ratio into the base carrier liquid container heated in step 2, and stir fully with a stirring rod to completely dissolve the surfactant mixture in the base carrier liquid,...

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Abstract

The invention discloses non-aqueous magnetorheological polishing fluid which is steady at low viscosity and a preparation method thereof. The non-aqueous magnetorheological polishing fluid comprises basic carrier fluid which accounts for 40 to 75 percent of the total volume of the magnetorheological polishing fluid, 15 to 50 percent of carbonyl iron powder, 3 to 8 percent of surfactant and 3 to 6 percent of polishing powder, wherein, the basic carrier fluid is dimethicone. The preparation method of the invention is as follows: the surfactant is completely dissolved in the basic carrier fluid by heating and stirring, then the magnetic granular carbonyl iron powder and the basic carrier fluid mixture are mixed, then a ball-grinding device of a ball grinder is adopted to disperse the mixture so as to improve the anti-sedimentation property and the stability of the magnetorheological polishing fluid to finally ensure that the prepared magnetorheological polishing fluid always keeps rolling to maintain the stability of the characteristic of the magnetorheological polishing fluid. The polishing fluid prepared by the invention has low zero magnetic field viscosity, big shear yield stress and good magnetorheological performance, is suitable for the processing of deliquescent optical materials, and has a simple preparation process, no toxicity, and low cost.

Description

technical field [0001] The invention belongs to magnetorheological polishing of optical parts, in particular to a low-viscosity stable non-water-based magnetorheological polishing liquid and a preparation method thereof. Background technique [0002] Magneto-rheological polishing technology is a new type of optical processing method. It uses the rheology of magnetorheological polishing fluid in a magnetic field to polish optical parts, which can achieve deterministic removal and sub-nanometer surface roughness. Among them, magnetorheological The performance of the polishing fluid directly determines the effect of magnetorheological polishing, and is a key component of magnetorheological polishing technology. According to the processing characteristics of magnetorheological polishing technology, the main performance requirements for magnetorheological polishing fluid are: low zero magnetic field viscosity, magnetorheological polishing fluid can circulate in the circulation eq...

Claims

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Application Information

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IPC IPC(8): C09G1/16C09G1/02H01F1/44
Inventor 李圣怡彭小强戴一帆陈浩锋王贵林吴宇列尹自强
Owner NAT UNIV OF DEFENSE TECH
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