Conjugated polymer bulk heterojunction film with optical anisotropy and preparation method and application thereof
An optically anisotropic, conjugated polymer technology, used in semiconductor/solid-state device manufacturing, photovoltaic power generation, electric solid-state devices, etc., can solve the problems of difficult assembly, weak interaction force, etc., and achieve a simple and simplified preparation method. The effect of simple design and experimental conditions
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[0053] 1) First, dissolve 10mg of P-type TQ1 (Mn=71KDa) in 1ml of chloroform to obtain solution X, then dissolve 10mg of N-type N2200 (Mn=100-150KDa, PDI 3.0-4.5) in 1ml of chloroform to obtain For solution Y, prepare solution Z by mixing solution X and Y at a volume ratio of 2:1, shake the solution, seal it and place it at room temperature for use. The molecular structure of the material is as figure 2 shown.
[0054] 2) Inject an appropriate amount of the above-mentioned mixed solution Z onto the surface of the ethylene glycol liquid at a rate of 7mL / h by using a slot die print head with a straight opening, so that the mixed solution Z spreads on the ethylene glycol liquid surface to form a high-quality uniform thickness band Self-assembled optically anisotropic active layer thin film; transferring this thin film from liquid surface to ITO / TiO using the Langmuir-Blodgett (LB) method 2 On the substrate of the electron transport layer; place the transferred substrate at 100...
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