Wormwood PE functional master batch and application thereof in plastic products

A technology of wormwood and antibacterial masterbatch, which is applied in the field of wormwood PE functional masterbatch and its application in plastic products. It can solve the problems of unstable quality and composition change of PE masterbatch, achieve good release and improve antibacterial performance , improve the effect of strength

Pending Publication Date: 2020-12-29
BYHERB BIGBIO TECH QINGDAO CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The above patent is to directly add functional ingredients into the preparation process of PE masterbatch, and finally make a functional PE masterbatch. With the public's recognition of traditional Chinese medicine technology, many manufacturers in the industry adopt plants that will have the effect of traditional Chinese medicine. The extract is added to the preparation process of PE masterbatch to make PE masterbatch containing plant extracts to achieve the functionality of some plant extracts. However, due to the high temperature of PE masterbatch in melting, it is easy to add ingredients Changes occur under the action of high temperature, resulting in unstable quality of the prepared PE masterbatch, so the inventor thought of adding functional components to the PE masterbatch by porous adsorption, and the present invention is based on this

Method used

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  • Wormwood PE functional master batch and application thereof in plastic products
  • Wormwood PE functional master batch and application thereof in plastic products
  • Wormwood PE functional master batch and application thereof in plastic products

Examples

Experimental program
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Effect test

Embodiment 1

[0034] Embodiment 1 A kind of preparation method of wormwood PE functional masterbatch, comprising:

[0035] The present invention firstly provides a kind of mugwort PE antibacterial masterbatch, comprises following raw material composition:

[0036] PE resin chip 80%, filler 5%, dispersant 2%, modifier 3%, antibacterial active molecular nest 10%, antibacterial active molecular nest is made of wormwood extract and titanium dioxide macromolecular nest matrix; titanium dioxide macromolecular nest The preparation method of the matrix includes: the steps of precursor solution preparation, solvent volatilization, and titanium dioxide macromolecular nest matrix formation;

[0037] Precursor solution preparation includes:

[0038] Add a certain amount of F127, deionized water, formic acid, HCl to THF in turn, add fixative and stabilizer, stir magnetically for 40min to dissolve completely, and form a clear and transparent solution. Under vigorous magnetic stirring, add TBOT and The ...

Embodiment 2

[0053] Embodiment 2 A kind of mugwort PE functional masterbatch and its preparation method, comprising:

[0054] The present invention firstly provides a kind of mugwort PE antibacterial masterbatch, comprises following raw material composition:

[0055] PE resin chip 90%, filler 5%, dispersant 1%, modifier 1%, antibacterial active molecular nest 3%, antibacterial active molecular nest is made of wormwood extract and titanium dioxide macromolecular nest matrix; titanium dioxide macromolecular nest The preparation method of the matrix includes the steps of preparing a precursor solution, volatilizing a solvent, and forming a titanium dioxide macromolecular nest matrix.

[0056] Precursor solution preparation includes:

[0057] Add a certain amount of F127, deionized water, formic acid, HCl to THF in turn, add fixative and stabilizer, stir magnetically for 60 minutes to dissolve completely, and form a clear and transparent solution. Under vigorous magnetic stirring, add TBOT an...

Embodiment 3

[0071] Embodiment 3 A kind of mugwort PE functional masterbatch and its preparation method, comprising:

[0072] The present invention firstly provides a kind of mugwort PE antibacterial masterbatch, comprises following raw material composition:

[0073] PE resin chip 85%, filler 5%, dispersant 2%, modifier 3%, antibacterial active molecular nest 7%, antibacterial active molecular nest is made of wormwood extract and titanium dioxide macromolecular nest matrix; titanium dioxide macromolecular nest The preparation method of the matrix includes the steps of preparing a precursor solution, volatilizing a solvent, and forming a titanium dioxide macromolecular nest matrix.

[0074] Precursor solution preparation includes:

[0075] Add a certain amount of F127, deionized water, formic acid, HCl to THF in sequence, add fixative and stabilizer, stir magnetically for 70 minutes to dissolve completely, and form a clear and transparent solution. Under vigorous magnetic stirring, add TBO...

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Abstract

The invention relates to the technical field of PE master batches, in particular to a wormwood PE antibacterial master batch which is prepared from the following raw materials: 80-90% of PE resin slices, 5-15% of filler, 1-5% of dispersing agent, 1-3% of modifier and 3-10% of antibacterial active molecular nest, and the antibacterial active molecular nest is prepared from wormwood extract and titanium dioxide macromolecular nest matrix; the preparation method of the titanium dioxide macromolecular nest matrix comprises the following steps: preparing a precursor solution, volatilizing a solvent, and forming the titanium dioxide macromolecular nest matrix. The particle size of the antibacterial active molecular nest is 800-1000nm, the pore diameter is 8-15nm, and the specific surface area is650-800m<2> / g. The wormwood PE antibacterial master batch prepared by the method shows very good antibacterial property, and the staphylococcus aureus antibacterial rate, escherichia coli antibacterial rate and pseudomonas aeruginosa antibacterial rate are all greater than or equal to 99.9%.

Description

technical field [0001] The invention relates to the technical field of PE master batches, in particular to a mugwort PE functional master batch and its application in plastic products. Background technique [0002] PE masterbatch, the chemical name is polyethylene plastic, one of the most commonly used polymer materials, its performance is very stable, it is a non-toxic and environmentally friendly material, plastic products, plastic films, plastic bags, food bags, protective Films and electrostatic films are all made of this material. [0003] Patent CN201811455179.4 discloses a plant-derived PE masterbatch, which is mainly prepared by blending and melting PE masterbatch and modified motherwort extract; the PE masterbatch and the modified motherwort The mass ratio of the extract is 99:21; the plant-derived PE masterbatch prepared by the present invention has regular shape, no conjoined particles, no debris, particle size uniformity of 93.2-94.9%, and melt flow rate of 4.4-...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/06C08K9/12C08K5/00C08K7/24C08K3/26C08K5/521C08K13/06C08J3/22
CPCC08J3/226C08J2423/06C08J2300/00C08K9/12C08K5/0058C08K7/24C08K2003/265C08K5/521C08K13/06C08K2201/003C08K2201/006
Inventor 黄效华刘健汪培育刘建国王爽原秀燕
Owner BYHERB BIGBIO TECH QINGDAO CO LTD
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