Multi-functional reusable mask for efficient filtration and adsorption sterilization and preparation method thereof
A high-efficiency filtration and multi-functional technology, applied in the field of sanitary protection products, to achieve the effect of high porosity, low density and high adsorption capacity
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[0032] Wherein, the preparation method of silver ion-doped titanium dioxide-coated attapulgite-oxide nanofiber layer comprises the following steps:
[0033] 1) At least one of alumina sol, silica sol, yttrium oxide sol and zirconia sol is selected as the oxide precursor sol, and mixed with water at a volume ratio of 1:(1-3), and then added with a molecular weight of 8-130×10 4 At least one of PVA, PVP or PEO is mixed as a spinning aid and magnetically stirred for 4-24h to obtain a spinnable ceramic precursor sol; wherein, the quality of the oxide and spinning aid in the oxide precursor sol The ratio is 100:(5-20);
[0034] 2) Spinnable ceramic precursor sol is placed in high-voltage electrospinning equipment for spinning to obtain oxide precursor fiber film; wherein, the spinning conditions include: spinning voltage of 12-25kV, spinning distance of 10 -30cm, the spinning temperature is 20-40℃, and the injection speed is 0.3-2mL / h;
[0035] 3) Sintering the oxide precursor f...
Embodiment 1
[0041] A method for preparing a multi-functional reusable mask for high-efficiency filtration and adsorption and sterilization, using non-woven fabric as the first support layer, silver ion-doped titanium dioxide-coated attapulgite-oxide nanofiber layer as the multi-functional layer, no The woven fabric is used as the second supporting layer to be stacked and placed in sequence, and then after being cut and edge-pressed and connected in sequence, the above-mentioned mask can be obtained.
[0042] Wherein, the preparation method of silver ion-doped titanium dioxide-coated attapulgite-oxide nanofiber layer comprises the following steps:
[0043] 1) Add 20mL of alumina sol to 20mL of deionized water, then add4 The PVP is mixed and magnetically stirred for 8h as a spinning aid to obtain a spinnable ceramic precursor sol; wherein, the mass ratio of the spinning aid to alumina is 1:10;
[0044] 2) Spinnable ceramic precursor sol is placed in high-voltage electrospinning equipment fo...
Embodiment 2
[0050] A method for preparing a multi-functional reusable mask for high-efficiency filtration and adsorption and sterilization, using non-woven fabric as the first support layer, silver ion-doped titanium dioxide-coated attapulgite-oxide nanofiber layer as the multi-functional layer, no The woven fabric is used as the second supporting layer to be stacked and placed in sequence, and then after being cut and edge-pressed and connected in sequence, the above-mentioned mask can be obtained.
[0051] Wherein, the preparation method of silver ion-doped titanium dioxide-coated attapulgite-oxide nanofiber layer comprises the following steps:
[0052] 1) Add 20mL of alumina sol to 30mL deionized water, then add 4 The PVP was mixed and magnetically stirred for 8h as a spinning aid to obtain a spinnable ceramic precursor sol; wherein, the mass ratio of the spinning aid to alumina was 13:100;
[0053] 2) Spinnable ceramic precursor sol is placed in high-voltage electrospinning equipment...
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