Furyl double-long-chain quaternary ammonium salt compound as well as preparation method and application thereof

A quaternary ammonium compound and double long-chain technology, applied in the field of disinfectants, can solve the problems of poor biodegradability, strong irritation, and damage to human health of disinfectants, and achieve strong bactericidal effect, high-efficiency killing effect, and rapid sterilization The effect of the killing effect

Active Publication Date: 2022-07-15
ZHONGYUAN ENGINEERING COLLEGE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] (1) Traditional disinfectants are highly irritating, and long-term use is detrimental to human health;
[0006] (2) Traditional disinfectants have the disadvantage of poor biodegradability

Method used

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  • Furyl double-long-chain quaternary ammonium salt compound as well as preparation method and application thereof
  • Furyl double-long-chain quaternary ammonium salt compound as well as preparation method and application thereof
  • Furyl double-long-chain quaternary ammonium salt compound as well as preparation method and application thereof

Examples

Experimental program
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preparation example Construction

[0072] An embodiment of the present invention provides a method for preparing a furan-based double long-chain quaternary ammonium salt compound, comprising: using the obtained double-long-chain secondary amine intermediate product K to react with a chloroethane reagent V to obtain the furan-based double-long-chain quaternary ammonium salt salt compound.

[0073] Double long chain secondary amine intermediate product K, the structural formula is shown in the figure below;

[0074]

Embodiment 1

[0076] The embodiment of the present invention provides a furan-based double long-chain quaternary ammonium salt compound, the furan-based double long-chain quaternary ammonium salt compound is selected from compounds having the structural formula shown in formula I, and the compound is a caramel-colored viscous liquid, which is easy to Soluble in water and alcohol solvents;

[0077]

[0078] Its structure contains two quaternary ammonium salt substituents.

[0079] The substituents on the nitrogen atom of the quaternary ammonium salt group are one C12 alkyl long chain and two ethyl functional groups, and the anion is chloride ion.

Embodiment 2

[0081] Based on the furanyl double long-chain quaternary ammonium salt compound provided in Example 1 of the present invention, such as figure 1 As shown, the embodiment of the present invention provides a preparation method of a furanyl double long-chain quaternary ammonium salt compound, comprising the following steps:

[0082] S101, the mixture containing compound i and compound ii is reacted with I in the presence of a basic substance or an acidic substance to obtain the imine compound P, whose structural formula is shown in the following figure;

[0083]

[0084] S102, the imine compound P is mixed with a reducing reagent to carry out reaction II to obtain a double long-chain secondary amine intermediate product K, the structural formula is as shown in the following figure;

[0085]

[0086] S103, the double long-chain secondary amine intermediate product K is reacted with a chloroethane reagent V to obtain the furanyl double long-chain quaternary ammonium salt comp...

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Abstract

The invention belongs to the technical field of disinfectants, and discloses a furyl double-long-chain quaternary ammonium salt compound as well as a preparation method and application thereof. The preparation method of the furyl double-long-chain quaternary ammonium salt compound comprises the following steps: carrying out a reaction I on a mixture containing a compound i and a compound ii in the presence of an alkaline substance or an acidic substance to obtain an imine compound P; mixing the imine compound P with a reducing reagent for reaction II to obtain a double-long-chain secondary amine intermediate product K; or the compound III reacts with the compound III in the presence of a halogenating reagent to obtain the chlorinated compound O; the chlorinated compound O and a compound i are mixed to react IV, and a double-long-chain secondary amine intermediate product K can be obtained; and reacting the double-long-chain secondary amine intermediate product K with a chloroethane reagent V to obtain the furyl double-long-chain quaternary ammonium salt compound. The furyl double-long-chain quaternary ammonium salt compound disclosed by the invention has a rapid killing effect on bacterial propagules as an organic disinfectant.

Description

technical field [0001] The invention belongs to the technical field of disinfectants, and in particular relates to a furan-based double long-chain quaternary ammonium salt compound, a preparation method and its application as a disinfectant. Background technique [0002] In order to strengthen personal hygiene protection and reduce new coronavirus infection, the development of efficient, safe and green disinfectant products is a common concern of the society. [0003] Compared with traditional chlorine-containing disinfectants and peroxide disinfectants, quaternary ammonium salt type disinfectants have the advantages of low toxicity, less odor, convenient use, and easy storage. They are very suitable for use as household disinfection products. [0004] Through the above analysis, the existing problems and defects in the prior art are: [0005] (1) Traditional disinfectants are highly irritating, and long-term use is detrimental to human health; [0006] (2) Traditional dis...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D307/52A01N43/08A01P1/00
CPCC07D307/52A01N43/08
Inventor 艾文英杨宇刘国群李鹏宇冯世龙刘柯心张甜张梦真刘一帆钟文涛
Owner ZHONGYUAN ENGINEERING COLLEGE
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