Method of painting flourous delayed releasing matter onto denture to preventing demineralization of enamel
An orthodontic bracket and tooth enamel technology, applied in dentistry, dental preparations, dental prostheses, etc., can solve problems such as inconvenient operation, and achieve the effects of convenient operation, long release time, and prevention of enamel demineralization
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Embodiment 1
[0024] Choose CaF 2 As the coating material, a magnetron sputtering method is used. CaF 2 The powder was ball milled in a ball mill with a speed of 300 rpm for 24 hours, pressed into a Φ60*5 disc, sintered at a high temperature of 1250°C to make a target, and then sputtered on the surface of the orthodontic bracket by radio frequency magnetron sputtering. Sputtering conditions The frequency is 13.56MHz, the sputtering power is 250W, the working argon pressure is 1.5Pa, the target base distance is 65mm, and the sputtering is 3 hours, that is, the CaF-containing 2 slow-release coating.
Embodiment 2
[0026] Choose MgF 2 As a coating material, a sol-gel method is used. MgF 2 Make a sol, immerse the orthodontic bracket in the sol, pull it at a speed of 0.1mm / min, then dry it at 100°C for 1 hour, and heat it at 650°C for 3 hours to get the MgF-containing 2 slow-release coating.
Embodiment 3
[0028] The fluorine-containing hydroxyapatite is selected as the coating material, and the sol-gel method is adopted. First, fluorine-containing hydroxyapatite is made into a sol, and the orthodontic bracket is immersed in the sol, pulled at a speed of 0.5mm / min, then dried at 200°C for 2 hours, and heat-treated at 300°C for 1 hour to obtain fluorine-containing hydroxyapatite Apatite slow-release coating.
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