Stabilized virus-like particles and epitope display systems
A virus and epitope technology, applied in the interdisciplinary field of immunology and peptide engineering, can solve problems such as immune interference
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Embodiment 1
[0289] Example 1: Construction of stabilized HBc polypeptide VLP with M2 ectodomain
[0290] To illustrate the ability of the N-terminal region of the influenza virus M2 protein to non-covalently stabilize hepatitis B virus core-like particles, the extracellular domain of M2e was fused to the C-terminus of a C-terminally truncated HBc polypeptide. To ensure that no intrinsic cysteine residues contributed to the stabilization, a version of M2 (positions 2-24) in which cysteines were mutated to serines was used (CV-1895, V7.M2e (2C > 2S). The expression vector V7.M2e (2C>2S) was constructed, and a pair of oligonucleotides were annealed and inserted into the expression vector V7 (see below), and the vector V7 accepted the insertion after the amino acid V149 of the HB capsid polypeptide gene. This is shown in Fig. 2 is shown schematically.
[0291] Therefore, a new vector was constructed to enable the fusion of the self-binding peptide to the C-terminus of the HBc chimera. Uni...
Embodiment 2
[0305] Example 2: Analysis of Stabilized HB Capsid Polypeptide VLP
[0306] After expression and purification of the particles, their ability to maintain particle-like morphology was analyzed by analytical size-exclusion chromatography. When analyzed in this manner, non-C-terminally stabilized particles (eg, CV-1048) were present as a mixture of particulate and non-particulate material.
[0307] Similar analysis of the CV-1895 particles revealed that they elute as a uniform particle structure ( Figure 4 ). These data suggest that the M2e(2-24, C17S, C19S) sequence, when present, fuses to the C-terminus of HBc, forming an intermolecular interaction that stabilizes the granular structure. These data further suggest that intermolecular stabilization occurs in the absence of cysteine residues at positions 17 and 19 of M2.
Embodiment 3
[0308] Example 3: Construction of stabilized HBc polypeptide VLP with GCN4-p1 leucine zipper
[0309] In order to study the ability of the leucine zipper domain of the yeast GCN4 transcriptional regulator to stabilize hepatitis B capsid polypeptide particles in a non-covalent manner, a protein derived from GCN4 that can simultaneously form dimers and trimers in solution The modified leucine zipper GNC4-VL of the body was fused to the C-terminus of the C-terminal truncated HBc particle by genetic engineering. According to the method for constructing the expression vector in Example 1, the synthetic oligonucleotide encoding GCN4-VL was annealed and inserted into the expression vector V7, and the vector V7 was inserted after amino acid V149 of the HB capsid polypeptide gene. The peptide linked to the HB capsid in this way has the following sequence:
[0310] RVKQLEDKVEELLSKVYHLENEVARLKKLVGER
[0311] SEQ ID NO: 282
[0312] The obtained particles are more s...
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