Puerarin monocrystal and preparation method thereof
A technology of puerarin and single crystal, applied in the direction of organic chemistry, etc., can solve the problems such as the method and crystal structure data of puerarin single crystal that have not been clearly obtained.
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Embodiment 1
[0050] Weigh 0.5g of puerarin raw material into a beaker, add 8ml of methanol solvent to dissolve, seal the beaker, add 1mg of seed crystals, let stand at 20°C for 2-3 days, filter and dry to obtain needle crystals or long columnar crystals.
[0051] The crystal X-single crystal diffraction data are the same as the attached page.
Embodiment 2
[0053] Weigh 1.0g of puerarin raw material into a beaker, add 19ml of ethanol solvent, dissolve at a slight temperature, seal the beaker, let stand at 0°C for 2-3 days, filter and dry to obtain columnar crystals or square crystals.
[0054] The crystal X-single crystal diffraction data are the same as the attached page.
Embodiment 3
[0056] Weigh 1.0g puerarin raw material in a beaker, add 19ml ethanol-H 2 Mix O with a solvent, dissolve at a slight temperature, seal the beaker, let stand at 4°C for 2-3 days, filter and dry to obtain columnar crystals or square crystals.
[0057] The crystal X-single crystal diffraction data are the same as the attached page.
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