Method for quickly synthesizing ferric stearate
A technology of iron stearate and stearic acid, applied in carboxylate preparation, organic chemistry, etc., can solve problems such as low product yield, poor quality, and influence on reaction, and achieve high purity, low energy consumption, and simple process Effect
Inactive Publication Date: 2013-03-27
QINGDAO SHUAIWANG OIL CHEM
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Problems solved by technology
[0002] Iron stearate can be used as plastic photosensitizer, and its synthetic method mainly adopts saponification-metathesis method, and this method needs to add a large amount of lye, thereby generates a large amount of salt waste liquid, and iron stearate in reaction process It is easy to float on the liquid surface, affecting the progress of the reaction, resulting in low product yield and poor quality
Method used
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Experimental program
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Effect test
Embodiment 1
[0009] Stearic acid, ferric oxide and ferric oxide are mixed uniformly in a mass ratio of 50:30:20, and 10% of the total weight of the compound is added as catalyst ethylene bis stearamide and paraffin hydrocarbon, ethylene bis stearamide and paraffin hydrocarbon The mass ratio of the mixture was 1:9, and reacted at 70° C. for 2 hours to obtain the iron stearate mixture.
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The invention discloses a method for quickly synthesizing ferric stearate, which comprises the following steps of: directly adopting stearic acid, ferric oxide and ferric trioxide as raw materials; adding a catalyst; and then reacting at 70 DEG C for 2 hours to obtain a ferric stearate mixture. The method disclosed by the invention has the advantages of no alkali liquor addition, little production waste liquor, simple process, low energy consumption and high ferric stearate purity.
Description
technical field [0001] The invention belongs to the technical field of organic compound synthesis, in particular to a method for rapidly synthesizing iron stearate. Background technique [0002] Iron stearate can be used as plastic photosensitizer, and its synthetic method mainly adopts saponification-metathesis method, and this method needs to add a large amount of lye, thereby generates a large amount of salt waste liquid, and iron stearate in reaction process It is easy to float on the liquid surface, affecting the progress of the reaction, resulting in low product yield and poor quality. Contents of the invention [0003] For solving above technical problem, the object of the present invention is to provide a kind of method of fast synthetic iron stearate. [0004] The method of the present invention adopts the following technical scheme: stearic acid, ferric oxide and ferric oxide are mixed evenly in a mass ratio of 50:30:20, and after adding a catalyst, they are rea...
Claims
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Login to View More IPC IPC(8): C07C53/126C07C51/41
Inventor 王明夫
Owner QINGDAO SHUAIWANG OIL CHEM
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