Hot solidification type component used for filling printed circuit board punched hole
A printed circuit board, thermal curing technology, applied in the direction of the electrical connection of printed components, etc., can solve the problems of difficult processing, general products without suitable structure, and inability to fully take into account the combination and mechanical properties
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Synthetic example
[0046] [Synthetic reactive rubber]
[0047] The synthetic steps of reactive rubber are as follows:
[0048] (1) 10g of carboxy-terminated nitrile rubber and 20g of 4,4'-diaminodicyclohexylmethane were dissolved in 60mL of xylene to obtain a mixed solution.
[0049] (2) The mixture was heated to 110° C. under stirring, and reacted for 3 hours to obtain a reactive rubber.
[0050] (3) After the reactive rubber is cooled, confirm the carboxyl absorption peak (3300cm -1 Nearby OH broad absorption), and the disappearance of the amide bond (3300cm -1 The generation of elongated NH peak absorption nearby).
Embodiment 1
[0052] 45 g of bisphenol A diglycidyl ether oligomer, 5 g of poly(oxyethylene) diamine, 5 g of the reactive rubber of the synthesis example, and 11 g of calcium carbonate particles were fully kneaded to obtain thermosetting composition a1.
Embodiment 2
[0054] After fully kneading 30g of bisphenol A diglycidyl ether oligomer, 18g of poly(oxyethylene) diamine, 10g of the reactive rubber of the synthesis example and 23.2g of calcium carbonate particles, a thermosetting composition a2 is obtained
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