Preparation technology of cochineal pigment with colorful effect
A technology of cochineal red and preparation process, which is applied in the directions of inorganic pigment processing, organic dyes, fibrous fillers, etc., can solve problems such as not involving the application field of cochineal red, and achieve the effect of high looseness
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Embodiment 1
[0037] The pearl red pearlescent pigment FWD215 was used as the transparent flake substrate to prepare cochineal pigment. Its preparation steps are:
[0038] a. Dissolve cochineal in deionized water to make 30mL of cochineal solution with substrate coating rate of 1.5% and mass concentration of 15g / L;
[0039] b. Dissolve aluminum trichloride in deionized water to prepare 30 mL of aluminum trichloride solution with a molar concentration of aluminum ions of 0.13 mol / L;
[0040] c. Put 30g of pearl red pearlescent pigment with an average particle size of 10-60μm into the reactor, add 450mL of deionized water, stir and heat up to 25°C, adjust the pH value to 6.3 with hydrochloric acid solution, and make a suspension;
[0041] d. Pump carmine solution and aluminum chloride solution into the reactor in parallel with a constant flow pump, and use 0.5mol / L sodium hydroxide solution to keep the pH constant, and add cochineal red at the same time within 2 to 3 hours solution and alum...
Embodiment 2
[0044] The pearl red pearlescent pigment FWD215 was used as the transparent flake substrate to prepare cochineal pigment. Its preparation steps are:
[0045] a. Dissolving cochineal in deionized water to prepare 40 mL of cochineal solution with a substrate coating rate of 2.0% and a mass concentration of 15 g / L;
[0046] b. Dissolve aluminum trichloride in deionized water to prepare 40 mL of aluminum trichloride solution with a molar concentration of aluminum ions of 0.13 mol / L;
[0047] c. Put 30g of pearl red pearlescent pigment with an average particle size of 10-60μm into the reactor, add 450mL of deionized water, stir and heat up to 25°C, adjust the pH value to 6.3 with hydrochloric acid solution, and make a suspension;
[0048] d. Pump carmine solution and aluminum chloride solution into the reactor in parallel with a constant flow pump, and use 0.5mol / L sodium hydroxide solution to keep the pH constant, and add cochineal red at the same time within 2 to 3 hours soluti...
Embodiment 3
[0051] The pearl red pearlescent pigment FWD215 was used as the transparent flake substrate to prepare cochineal pigment. Its preparation steps are:
[0052] a. Dissolve cochineal in deionized water to make 50mL of carmine solution with substrate coating rate of 2.5% and mass concentration of 15g / L;
[0053] b. Dissolve aluminum trichloride in deionized water to prepare 50 mL of aluminum trichloride solution with a molar concentration of aluminum ions of 0.13 mol / L;
[0054] c. Put 30g of pearl red pearlescent pigment with an average particle size of 10-60μm into the reactor, add 450mL of deionized water, stir and heat up to 25°C, adjust the pH value to 6.3 with hydrochloric acid solution, and make a suspension;
[0055] d. Pump carmine solution and aluminum chloride solution into the reactor in parallel with a constant flow pump, and use 0.5mol / L sodium hydroxide solution to keep the pH constant, and add cochineal red at the same time within 2 to 3 hours solution and alumin...
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