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Production method and device for ametryn

A production method and technology for amethine are applied in the field of production methods and devices of amethine, and can solve the problems of unstable product quality, high energy consumption, long processing time, etc., and achieve automatic control, reduction of equipment investment, and reduction of The effect of energy consumption

Active Publication Date: 2015-01-07
NINGXIA G R FINE CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The above two methods are to wash the organic phase with water and distill it, and there are disadvantages such as high energy consumption, long processing time and unstable product quality in the process of processing.

Method used

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  • Production method and device for ametryn
  • Production method and device for ametryn

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Embodiment Construction

[0017] like figure 1 As shown, in the present invention, the scraper evaporator includes a first-level scraper evaporator 11, a second-level scraper evaporator 12, and a third-level scraper evaporator 13 (the evaporation area is 10 square meters), and the first-level scraper evaporator 11. The secondary scraped evaporator 12 and the tertiary scraped evaporator 13 are connected in series, arranged from top to bottom.

[0018] A material flow pipeline 2 is provided between the first-stage scraper evaporator 11 and the second-stage scraper evaporator 12, and the first-stage scraper jacket gas phase pipeline 4 is connected to the first-stage scraper evaporator 11, and the third-stage scraper evaporator 13 is connected with product transfer pipeline 6.

[0019] In order to reduce energy loss, equipment and pipelines are insulated.

[0020] like figure 2 As shown, the first-stage scraper evaporator is equipped with a special jacket, and the inside of the jacket is finned. The he...

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Abstract

The invention provides a production method and device for ametryn, and solves the technical problems of high energy consumption and low productivity in the production process of the ametryn. The production method comprises the following steps: dissolving the ametryn in an organic solvent to obtain an ametryn synthetic solution, and treating the ametryn synthetic solution by using a scraper evaporator to obtain an ametryn molten solution. The production device comprises the scraper evaporator; the scraper evaporator comprises a first-stage scraper evaporator, a second-stage scraper evaporator and a third-stage scraper evaporator which are connected in series. The production method device can be widely applied to the production field of s-triazine herbicide type products.

Description

technical field [0001] The invention relates to a production method and device of a herbicide, in particular to a production method and device of ametryn. Background technique [0002] At present, there are two main types of recognized production of arazine: one uses atrazine and sodium methyl mercaptide as raw materials to produce an organic solution of arazine in an organic solvent system; the other uses atrazine and sodium sulfate disulfide Methyl ester and the like are used as raw materials, and organic solvents are also used to obtain an organic solution of arazine after synthesis, such as the Chinese invention patent application whose publication number is CN101307030. [0003] The above two methods are to wash the organic phase with water and distill it, and there are disadvantages such as high energy consumption, long processing time, unstable product quality and the like in the process. Contents of the invention [0004] The purpose of the present invention is to...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07D251/52
Inventor 孙国庆侯永生迟志龙李志清张杰曾娇华焦宏琛王玲玲姜飞燕崔丽徐延磊朱宝仁付铭翟芳徐秀花
Owner NINGXIA G R FINE CHEM CO LTD