A Thermogravimetric Reactor for Large Sample Testing

A technology of reactors and high-temperature reactors, applied in instruments, material weighing, measuring devices, etc., can solve the problems of small sample quality and volume, unfavorable gas-solid reaction of sample vessels, etc., so as to avoid mutual influence and fully preheat , to avoid the effect of affecting

A technology of reactors and high-temperature reactors, applied in instruments, material weighing, measuring devices, etc., can solve the problems of small sample quality and volume, unfavorable gas-solid reaction of sample vessels, etc., so as to avoid mutual influence and fully preheat , to avoid the effect of affecting

CN103760054BInactive Publication Date: 2016-02-24HUAZHONG UNIV OF SCI & TECH

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  • A Thermogravimetric Reactor for Large Sample Testing
  • A Thermogravimetric Reactor for Large Sample Testing
  • A Thermogravimetric Reactor for Large Sample Testing

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Embodiment 2

[0066] Such as Figure 4 As shown, in Embodiment 2 of the present invention, thermogravimetric analysis is carried out on a large sample size particle sample, including a high temperature reactor 2, an electric heating furnace 1, a hydraulic lifting platform 3, a sealed box 4 and a gas source;

[0067] Such as figure 2 As shown, the high temperature reactor 2 is composed of an inner pipe 2-1 and an outer pipe 2-2, and the inner pipe 2-1 is composed of an integrated pipe body 2-11 and an expansion head 2-12 from bottom to top, The expansion head 2-12 is a rotating body, and its maximum diameter is larger than that of the pipe body 2-11. The bottom of the pipe body 2-11 has uniformly distributed holes, and the maximum diameter of the expansion head 2-12 has two symmetrical outlets. Gas port 2-12A, the pipe body 2-11 is located in the outer pipe 2-2, forming a coaxial sandwich casing structure, and the upper part of the outer pipe 2-2 has a reaction atmosphere inlet 2-2A;

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Abstract

The invention discloses a thermal gravimetrical reactor applied to bulk specimen testing, belonging to testing equipment for performing thermo gravimetric analysis on specimens and aiming to solve the problems that small-mass and small-sized specimens are required and a sample vessel is unbeneficial to gas-solid reactions in the conventional thermo gravimetric analyzer. Through a high-temperature reactor, reaction gas is preheated fully, so that mass measuring errors caused by temperature change of the reaction atmosphere are avoided; two types of hanging baskets are specific to different specimens respectively, so that the diffusion resistance during the reactions of bulk specimens is reduced effectively, and complete reactions and measuring accuracy are ensured; the height of an electric heating furnace is adjusted through a hydraulic lifting platform, so that samples can be heated at constant temperature under a high-accuracy condition. The thermal gravimetrical reactor can be used for dynamically measuring the mass changes of bulk specimens at various heating rates or under a constant-temperature condition, and is more consistent with the requirements of scientific research production than the conventional thermal gravimetrical analyzer.

Description

technical field [0001] The invention belongs to testing equipment for thermogravimetric analysis of samples, in particular to a thermogravimetric reactor for testing large samples, which can test the mass of large mass samples or large particle samples under programmed temperature rise or constant temperature heating conditions Variety. Background technique [0002] Thermogravimetric analysis is to make the sample under the preset heating conditions, and analyze the relationship between the mass of the sample and the change of temperature or time under the set reaction atmosphere. It is widely used in the study of the composition, thermal stability, oxidation and reduction, and adsorption of samples. and desorption, reaction kinetics, and the effects of additives and catalysts, etc. The existing thermogravimetric analyzer is generally composed of a balance, an electric furnace, a program temperature control system, a recording system and other components, and measures the m...

Claims

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Application Information

Patent Timeline
24 Feb 2016
Publication
CN103760054B
IPC
G01N5/00
Inventors
杨海平; 田路泞