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Y-type molecular sieve modification method and catalytic cracking catalyst preparation method

A molecular sieve and modification technology, which is applied in the direction of molecular sieve catalysts, catalytic cracking, physical/chemical process catalysts, etc., can solve the problem of poor effect of reducing sodium ion content, achieve stable roasting temperature, reduce energy consumption, and ensure the effect.

Active Publication Date: 2014-05-07
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0012] The purpose of the present invention is to overcome the problem of poor effect of reducing sodium ion content in the modification of Y-type molecular sieve and the preparation of catalytic cracking catalyst, and provide a modification method of Y-type molecular sieve and a preparation method of catalytic cracking catalyst

Method used

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  • Y-type molecular sieve modification method and catalytic cracking catalyst preparation method
  • Y-type molecular sieve modification method and catalytic cracking catalyst preparation method
  • Y-type molecular sieve modification method and catalytic cracking catalyst preparation method

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preparation example Construction

[0068] The present invention also provides a method for preparing a catalytic cracking catalyst, the method comprising: modifying a Y-type molecular sieve to obtain a modified Y-type molecular sieve, and taking the total weight of the catalytic cracking catalyst as a basis, adding 5-50% by weight of The modified Y-type molecular sieve, 0.5-50% by weight of the binder in terms of oxides and 5-90% by weight of the clay mixture are gelled, and the obtained gelled products are sequentially dried and roasted to obtain a roasted product, The roasting temperature of the dried gelled product is 350-400° C., and the roasted product is washed, filtered and dried in sequence. The washing of the roasted product is water washing, and the washing temperature of the roasted product is 20-400° C. 45°C, the weight ratio of the water used for washing the roasted product to the roasted product is 5-20:1; the method for modifying the Y-type molecular sieve is the modification of the Y-type molecul...

Embodiment 1

[0091] This example is used to illustrate the modification method of the Y-type molecular sieve of the present invention.

[0092] Add 50kg NaY molecular sieve (Qilu Catalyst Factory) to the beating tank with 400kg deionized water, add ammonium sulfate 150kg, the weight ratio of water and NaY molecular sieve is 8:1, the weight ratio of ammonium sulfate and NaY molecular sieve is 3:1, the first exchange is carried out in the beating tank, the exchange temperature is 80°C, and the exchange time is 2 hours. The exchanged NaY molecular sieves enter the flash dryer for drying, the drying temperature is 180° C., and the drying time is 1.5 hours.

[0093] The dried NaY type molecular sieve is put into a roasting furnace as a Y type molecular sieve to be roasted for roasting. roaster such as figure 2 shown. The inner diameter of the entire cylinder 2 is 1 m, the length of the entire cylinder 2 is 7 m, wherein the lengths of the feed end 24 and the discharge end 25 are 0.5 m, and t...

Embodiment 2

[0101] This example is used to illustrate the modification method of the Y-type molecular sieve of the present invention.

[0102]Add 50kg of NaY molecular sieve (Qilu Catalyst Factory) to the beating tank with 250kg of deionized water, add 35kg of ammonium sulfate, the weight ratio of water to NaY molecular sieve is 5:1, and the weight ratio of ammonium sulfate to NaY molecular sieve is 0.7:1, the first exchange is carried out in the beating tank, the exchange temperature is 100°C, and the exchange time is 1.5 hours. The exchanged NaY type molecular sieves enter the flash dryer for drying, the drying temperature is 200° C., and the drying time is 1 hour.

[0103] The dried NaY type molecular sieve is put into a roasting furnace as a Y type molecular sieve to be roasted for roasting. The roasting furnace in Example 1 was used, except that the outer diameter of the heat insulating member 5 was 10 cm.

[0104] The entire roasting furnace is placed with the axial direction of t...

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Abstract

The invention discloses a Y-type molecular sieve modification method and a catalytic cracking catalyst preparation method. The Y-type molecular sieve modification method is characterized in that: a furnace having a heat insulation part is used, improved roasting conditions and secondary exchange conditions are adopted, and the roasting temperature of a Y-type molecular sieve is 400-500DEG C; and the secondary exchange is water washing or acidic solution washing, and the secondary exchange temperature is 20-70DEG C. The Y-type molecular sieve prepared through the modification method has a low Na2O content, and a catalytic cracking catalyst prepared by using the modified Y-type molecular sieve has a good catalysis performance.

Description

technical field [0001] The invention relates to a modification method of a Y-type molecular sieve and a preparation method of a catalytic cracking catalyst. Background technique [0002] Catalytic cracking catalyst is an important secondary processing process in petroleum refining - the catalyst used in the catalytic cracking process. In catalytic cracking catalysts, Y-type molecular sieve is a very widely used material, and it is also a very important active component. The performance of Y-type molecular sieve directly affects the reaction performance of catalytic cracking catalyst. In order to improve the use effect of Y-type molecular sieve, according to different needs, different modifications can be made to Y-type molecular sieve to meet the requirements of use. Many technologies have proposed methods for modifying Y-type molecular sieves. [0003] Usually, in the preparation of catalytic cracking catalyst, the Na of catalytic cracking catalyst is required + The con...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B39/24B01J29/08C10G11/05
Inventor 周灵萍张蔚琳田辉平朱玉霞许明德张杰潇
Owner CHINA PETROLEUM & CHEM CORP
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