Copper powder composition and production method thereof
A composition and technology of copper powder, applied in the field of copper powder production, can solve the problem of not being able to meet the looseness and other problems, and achieve the effects of reducing consumption, uniform particle size and good forming performance
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[0034] Example 1
[0035] The preparation method of the copper powder composition of the present invention comprises the following steps:
[0036] The preparation method of electrolytic copper powder, comprising the following steps:
[0037] 1. Copper powder electrolysis: the anode is a cast copper anode plate, and the number of copper anodes is 13; the cathode is a cold-rolled cathode plate, and the number of cathodes is 12; the electrolyte is CuSO4 solution, copper ion: 5g / L; sulfuric acid: 110g / L, chloride ion: 0.5mg / L; electrolytic current density: 1000A / m 2 ; Electrolyte temperature: 45℃.
[0038] Scraping powder: Use a powder scraper to brush twice up and down, and scrape the powder once every 40 minutes.
[0039] 2. Washing powder: Use a 3-ton capacity filter washing machine to wash powder until BaCl is used. 2 Until no white precipitate is detected, the moisture content is controlled at 18%.
[0040] 3. Drying and reduction: steel belt furnace is used, and the ...
Example Embodiment
[0056] Example 2
[0057] The preparation method of the copper powder composition of the present invention comprises the following steps:
[0058] The preparation method of electrolytic copper powder, comprising the following steps:
[0059]1. Copper powder electrolysis: the anode is a cast copper anode plate, and the number of copper anodes is 13; the cathode is a cold-rolled cathode plate, and the number of cathodes is 12; the electrolyte is CuSO4 solution, copper ion: 8g / L; sulfuric acid: 160 g / L, chloride ion: 0.8mg / L; electrolytic current density: 1500A / m 2 ; Electrolyte temperature: 60℃.
[0060] Scraping powder: Use a powder scraper to brush twice up and down, and scrape the powder once every 40 minutes.
[0061] 2. Washing powder: Use a 3-ton capacity filter washing machine to wash powder until BaCl is used. 2 Until no white precipitate is detected, the moisture content is controlled at 22%.
[0062] 3. Drying and reduction: steel belt furnace is used, and the c...
Example Embodiment
[0078] Example 3
[0079] The preparation method of the copper powder composition of the present invention comprises the following steps:
[0080] The preparation method of electrolytic copper powder, comprising the following steps:
[0081] 1. Copper powder electrolysis: the anode is a cast copper anode plate, and the number of copper anodes is 13; the cathode is a cold-rolled cathode plate, and the number of cathodes is 12; the electrolyte is CuSO4 solution, copper ion: 6g / L; sulfuric acid: 130g / L, chloride ion: 0.4mg / L; electrolytic current density: 1300A / m 2 ; Electrolyte temperature: 50℃.
[0082] Scraping powder: Use a powder scraper to brush twice up and down, and scrape the powder once every 40 minutes.
[0083] 2. Washing powder: use a filter washing machine, wash the powder until BaCl is used 2 Until no white precipitate is detected, the moisture content is controlled at 20%.
[0084] 3. Drying and reduction: steel belt furnace is used, and the condition is c...
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