A kind of infrared spectrum detection method of bird's nest

An infrared spectrum and infrared spectrometer technology, which is applied in the field of bird's nest identification, can solve the problems of destroying the integrity and uniformity of bird's nest, being unsuitable for mass detection, and being easily affected by the environment. Analyse simple and fast effects

Active Publication Date: 2016-05-25
厦门市燕之屋丝浓食品有限公司
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the problems of this method are: 1. The KBr method is easily affected by the environment, and the operation is cumbersome during detection, so it is not suitable for large-scale detection; 2. The integrity and uniformity of the bird’s nest will be destroyed during sampling, which may cause uneven sampling of the bird’s nest Cause misjudgment; 3. There are differences in the peak position, peak shape and peak height of the characteristic peaks of bird's nests from different origins, which may cause misjudgment

Method used

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  • A kind of infrared spectrum detection method of bird's nest
  • A kind of infrared spectrum detection method of bird's nest
  • A kind of infrared spectrum detection method of bird's nest

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Embodiment 1

[0042] Identification of Bird's Nest by Infrared Spectroscopy

[0043] Materials and Reagents:

[0044] Distilled water, test samples: genuine bird’s nest (East Coast Maoyan), genuine bird’s nest (KUNINGSEKAILI), genuine bird’s nest (Maoyan House), genuine bird’s nest (Maoyan Zhongnanma District), genuine bird’s nest (Indonesian Maoyan) all enter and exit from Xiamen The Inspection and Quarantine Bureau went to Southeast Asia to collect on-site; the adulterated bird's nest was provided by the Xiamen Entry-Exit Inspection and Quarantine Bureau; agar, tapioca starch, gelatin, tremella and pigskin. All test samples can be purchased in the market.

[0045] instrument:

[0046] NicoletiS10 infrared spectrometer (Nicolet, USA), electronic balance (accurate to 0.0001g; Sartorious, Germany), electric heating plate, oven.

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Abstract

The invention discloses an infrared spectrum detection method of bird's nest. It is characterized in that infrared spectrum detection is adopted, and the steps are pre-processing the samples to be identified; setting technical parameters, collecting infrared spectra of samples through infrared spectrometer; judging whether the bird's nest is adulterated by calculating 1634? The peak height of the absorption peak near cm-1 is 1037? The ratio of the peak height of the absorption peak near cm-1; if the ratio is between 0.90 and 1.30, it is genuine bird’s nest; if it is outside this range, the sample is adulterated, and the farther away from the interval, the lower the content of genuine bird’s nest; 1730? cm-1 absorption peak, the sample may be mixed with oily compounds such as pigskin. The invention measures the total extract in the bird’s nest, the pretreatment method is simple, non-toxic, the detection speed is fast, the detection cost is low, and the uniformity of sample detection is maintained at the same time; it is suitable for large batches of bird’s nest samples from different sources, and the infrared spectrum has a good reproducible and highly specific.

Description

technical field [0001] The invention relates to the identification field of bird's nest, in particular to an infrared spectrum detection method of bird's nest. Background technique [0002] Infrared spectroscopy (Infrared Spectroscopy, IR) research began in the early 20th century. Since the advent of commercial infrared spectrometers in 1940, infrared spectroscopy has been widely used in organic chemistry research. Especially with the rapid development of computer technology, it has driven the digitalization of analytical instruments and the development of chemometrics. Chemometric methods have achieved good results in solving spectral information extraction and background interference. The unique characteristics make people pay more attention to the value of near-infrared spectroscopy. The application research of near-infrared spectroscopy in various fields has been carried out one after another. Noteworthy as an independent analysis technique. [0003] In organic molecul...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N21/3563
Inventor 林睿徐敦明郭思立曾琪周昱范群艳黄丹燕
Owner 厦门市燕之屋丝浓食品有限公司
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