A Negative Process-free Lithographic Plate
A process-free, lithographic printing technology, applied to the photoplate-making process of the patterned surface, photosensitive materials used in optical mechanical equipment, instruments, etc., can solve the problems of insufficient printing resistance, and achieve improved printing resistance and strong adsorption Function, the effect of preventing particle aggregation
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Synthetic example 1
[0063] Add 100 grams of IPDI, 7.6 grams of 50nm diameter nano SiO 2 (Hydroxyl value 1.9mmol / g) and 1g of dibutyltin dilaurate catalyst were added to a 500mL four-necked flask with thermometer, stirrer and nitrogen introduction device, 2 Under protection, the reaction was stirred at 60℃ for 8 hours, and the chemical titration method was used to determine the -NCO content no longer decreased. 220g PPG was added, and the temperature reaction was kept to reduce the one NCO content to 45%. 51.4g HEA was added and measured by infrared spectroscopy. The 2235cm-NCO characteristic absorption peak disappears completely. Get about 380.0 grams of SiO 2 / Polyurethane acrylic prepolymer B1.
Synthetic example 2
[0065] Add 100 grams of IPDI and 19.0 grams of nano-SiO with a diameter of 10 nm 2 And 1g of dibutyltin dilaurate catalyst were added to a 500mL four-necked flask equipped with a thermometer, agitator and nitrogen introduction device, in the N 2 Under protection, the reaction was stirred at 60℃ for 8h, and the chemical titration method was used to determine the -NCO content no longer decreased. 216.0g PPG was added, and the temperature reaction was kept to reduce the one NCO content to 45%. 50.0g HEA was added and measured by infrared spectroscopy. The 2235cm-NCO characteristic absorption peak disappears completely. Get about 385.0 g SiO 2 / Polyurethane acrylic prepolymer B2.
Synthetic example 3
[0067] Add 100 grams of IPDI, 1.9 grams of nano SiO with a diameter of 100 nm 2 (Hydroxyl value 1.9mmol / g) and 1g of dibutyltin dilaurate catalyst were added to a 500mL four-necked flask with thermometer, stirrer and nitrogen introduction device, 2 Under protection, the reaction was stirred at 60℃ for 8 hours, and the chemical titration method was used to determine -NCO content no longer decreased. Add 224 grams of PPG, keep the temperature reaction to reduce the content of one NCO to 45%, add 52 grams of HEA, and measure by infrared spectroscopy The 2235cm-NCO characteristic absorption peak disappears completely. Get about 378.0 g SiO 2 / Polyurethane acrylic prepolymer B2.
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