Negative image flat printing plate precursor and method for fabricating flat printing plate
A lithographic and negative printing technology, applied in the field of negative lithographic printing plate precursors and the preparation of lithographic printing plates, can solve the problems of less number of papers to pass through the machine, high-quality dots, and inability to adapt to UV ink printing, etc., to achieve Good compatibility, improved printing resistance, strong adsorption effect
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Synthetic example 1
[0082] 168 gram of hexamethylene diisocyanate, 298 gram of pentaerythritol triacrylate and 1g of dibutyltin dilaurate catalyst were added in the 1000mL four-necked flask with thermometer, stirrer and nitrogen gas introduction device, under N 2 Under protection, stir and react at 60°C for 8 hours. The -NCO content is no longer decreased by chemical titration. Add 102 grams of N-methylolacrylamide and keep the temperature until the characteristic absorption peak of 2235cm-NCO measured by infrared spectroscopy disappears completely. About 570.0 g of urethane acrylic oligomer B1 containing amide groups was obtained.
Synthetic example 2
[0084] 168 gram of hexamethylene diisocyanate, 298 gram of pentaerythritol triacrylate and 1g of dibutyltin dilaurate catalyst were added in the 1000mL four-necked flask with thermometer, stirrer and nitrogen gas introduction device, under N 2 Under protection, stir and react at 60°C for 8 hours. Use the chemical titration method to determine that the -NCO content will no longer decrease. Add 164 grams of N-p-hydroxyphenylacrylamide and keep the temperature until the characteristic absorption peak of 2235cm-NCO measured by infrared spectroscopy disappears completely. . About 632.0 g of polyurethane acrylic oligomer B2 having amide groups were obtained.
Synthetic example 3
[0086] 168 gram of hexamethylene diisocyanate, 298 gram of pentaerythritol triacrylate and 1g of dibutyltin dilaurate catalyst were added in the 1000mL four-necked flask with thermometer, stirrer and nitrogen gas introduction device, under N 2 Stir and react at 60°C for 8 hours under protection. The -NCO content is no longer decreased by chemical titration. Add 178 grams of N-(p-hydroxyphenyl)methacrylamide, keep the temperature, and measure the characteristic absorption of 2235cm-NCO by infrared spectroscopy. until the peak disappears completely. This gives about 645.0 urethane acrylic oligomers B3 having amide groups.
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