A marine bacterium and its exopolysaccharide
A technology for marine bacteria and extracellular polysaccharides, applied in the field of extracellular polysaccharides, can solve problems such as limited bacterial polysaccharides
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Embodiment 1
[0027] The acquisition of embodiment 1 bacterial strain
[0028] Bacterial strain of the present invention obtains by following method screening: seawater is collected in August, 2012, longitude 115 ° E, latitude 18 ° N, depth of water 75m. Pipette 100 μL of the collected seawater onto the 2216E plate. 2216E medium: peptone 5.0g, yeast extract 1.0g, iron phosphate 0.01g, agar 20.0g, artificial seawater 1000ml, adjust ph to 7.6. Place at room temperature for incubation. After 3 days of culture, colonies with different shapes and sizes were randomly picked from the plate for purification and culture. When purifying, use an inoculation loop to pick colonies, and streak on the surface of the plate to observe whether the color, size, and shape of the strains on the plate are the same. Pick different colonies and streak until a colony of a single form is isolated. The polysaccharide-producing strain was detected by the phenol-sulfuric acid method to detect whether the culture sup...
Embodiment 2
[0032] The extraction of embodiment 2 polysaccharides
[0033] Determination of polysaccharide molecular weight
[0034] The molecular weight of polysaccharides was determined by high performance liquid chromatography. Polysaccharides were analyzed using a size exclusion column. Chromatographic column The column is made of TSK Gel GS3000SW XL Gel chromatography column (7.8mmID×30cm) and TSK GelG2000SW XL Gel chromatography columns (7.8mm ID×30cm) are connected in series, and the detector is a refraction detector. The mobile phase was 0.1 M ammonium acetate containing 0.2‰ sodium azide. The temperature of the column was set at 30° C., and the flow rate was set at 0.6 mL / min. Standard solutions include dextran (511, 167, 67, 40, 10, 5, 1 kDa) and maltotetraose (666.6 Da) with different molecular weights. Polysaccharides with different molecular weights have different retention times on size exclusion chromatography columns (see Table 1). According to the correlation betwe...
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