Anti-haze disinfecting mouth mask and preparation method
An anti-fog and mask technology, applied in protective clothing, clothing, clothing, etc., can solve the problems of loss of anti-virus, inability to wear masks, low adhesion, etc., to reduce adverse effects, broaden the frequency of light, and enhance antibacterial properties Effect
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[0029] The preparation method of the anti-smog mask of the present invention comprises the making of cover body and isolation filter, wherein the making of isolation filter is the key technology of the method of the present invention, and isolation filter is prepared according to the following steps:
[0030]a. Configure TiO2 sol: take absolute ethanol, tetrabutyl titanate, and water. The volume ratio of the above three substances is absolute ethanol: tetrabutyl titanate: water = 30:1:3, and the total amount of absolute ethanol Mix two-thirds of the amount with tetrabutyl titanate and stir evenly, mix the remaining amount of absolute ethanol with water and drop it into the mixture of absolute ethanol and tetrabutyl titanate, add acid solution to adjust the pH of the above mixture to 3. Continue to stir for 2 hours to prepare TiO2 sol.
[0031] b. Configure chitosan solution glue: configure chitosan solution glue according to the ratio of adding 1-5g chitosan and 5-25mg iodized...
Embodiment 1
[0040] Example 1: Take absolute ethanol, tetrabutyl titanate, and water according to the volume ratio of 30:1:3, mix and stir two-thirds of the total amount of absolute ethanol with tetrabutyl titanate, and mix the remaining After mixing water ethanol and water, drop it into the mixture of absolute ethanol and tetrabutyl titanate, add acid solution to adjust the pH of the above mixture to 3, and continue stirring for 2 hours to prepare TiO2 sol; according to 80ml acid solution and 20ml water , 1g chitosan and 5mg potassium iodide ratio configuration chitosan solution glue, the proportioning quantity potassium iodide and water are mixed to be uniform iodized salt water, the chitosan of proportioning quantity, acid solution and iodized salt water are mixed and stirred, Dissolve completely to chitosan, namely prepare into chitosan solution glue, described acid solution is the acetic acid of 1% mass concentration; Get prepared TiO Sol and chitosan solution glue, mix TiO according t...
Embodiment 2
[0041] Example 2: Take absolute ethanol, tetrabutyl titanate, and water according to the volume ratio of 30:1:3, mix and stir two-thirds of the total amount of absolute ethanol with tetrabutyl titanate, and mix the remaining After mixing water ethanol and water, drop it into the mixture of absolute ethanol and tetrabutyl titanate, add acid solution to adjust the pH of the above mixture to 3, and continue stirring for 2 hours to prepare TiO2 sol; according to 80ml acid solution and 20ml water Add 3g of chitosan and 10mg of ammonium iodide to configure chitosan solution gel, mix the proportioning amount of ammonium iodide with water to be uniform iodized salt water, and mix the proportioning amount of chitosan, acid solution and iodized salt Water mixes and stirs, dissolves completely to chitosan, promptly prepares chitosan solution glue, and described acid solution is the hydrochloric acid of 2% mass concentration; Get prepared TiO sol and chitosan solution glue, according to vo...
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