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A catalyst heavy metal circulation pollutes the aging reactor

A reactor and catalyst technology, applied in the field of reactors, can solve the problems of large water vapor consumption and long aging treatment time of aging reactors, and achieve the effects of simple structure, long treatment time and high reaction temperature

Active Publication Date: 2019-10-11
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] The purpose of the present invention is mainly to provide a catalyst heavy metal circulating pollution aging reactor to overcome the problems of large amount of steam in the aging reactor and long aging treatment time in the prior art

Method used

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  • A catalyst heavy metal circulation pollutes the aging reactor
  • A catalyst heavy metal circulation pollutes the aging reactor
  • A catalyst heavy metal circulation pollutes the aging reactor

Examples

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Embodiment 1

[0074] This example is used to illustrate the catalyst heavy metal recycling pollution aging reactor provided by the present invention and its application.

[0075] The stock oil used in this embodiment is Daqing straight-run diesel oil added with nickel naphthenate, vanadium naphthenate and iron naphthenate. In this diesel raw material, the content of nickel is 600ppm, the content of vanadium is 500ppm, and the iron content is 500ppm. The experimental device used is the heavy metal circulation pollution aging reactor device described in the present invention.

[0076] according to figure 1 The shown catalyst heavy metal cycle pollutes the aging reactor, and the reactor main body 11 includes a settling section III, an aging section II, and a pre-distribution section I from top to bottom, and the cross-sectional area of ​​the reactor main body 11 gradually decreases from top to bottom , the cross-sectional area of ​​the lower end of the settlement section III is equal to the ...

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Abstract

The invention discloses a catalyst heavy metal cycle pollution ageing reactor. The catalyst heavy metal cycle pollution ageing reactor comprises a reactor main body, a catalyst loading and unloading port, a feeding pipe, a gas outlet pipe, a grid, a spherical surface type tower plate and a gas inlet pipe; the reactor is divided into a settling section, an ageing section and a pre-distribution section from top to bottom; the cross sectional area of the reactor main body is shrunk from top to bottom; the grid is horizontally arranged at the ageing section of the reactor; the spherical surface type tower plate is arranged between the grid and the bottom end of the reactor; the feeding pipe passes through the upper part of the reactor and the grid and runs through the reactor to be positioned between the grid and the spherical surface type tower plate; the gas inlet pipe is arranged at the bottom of the reactor. The catalyst heavy metal cycle pollution ageing reactor provided by the invention is simple in structure, can flexibly switch hydrothermal ageing and heavy metal cycle pollution ageing, is simple in a cooling system, particularly adapts to requirements of high reaction temperature, large water vapor amount and long treatment time of cycle pollution ageing treatment, and can simulate the performance of an industrial balancing agent.

Description

technical field [0001] The invention relates to a reactor with stable activity of catalytic cracking catalyst in laboratory, more specifically, relates to a reactor for circularly polluting and aging treatment of catalytic cracking catalyst. Background technique [0002] Catalytic cracking technology is the main secondary processing technology of oil refining enterprises. The technology converts heavy hydrocarbon oil feedstocks into products such as gasoline, diesel, propylene and liquefied gas. [0003] During the operation of the catalytic cracking unit, metals such as iron, nickel, vanadium, and calcium in some heavy raw materials will contaminate the catalyst, reduce the activity of the catalyst, increase the content of heavy metals on the catalyst, and affect the performance of the catalyst and the distribution of its products. Therefore, in the research process of catalytic cracking catalyst and process, it is necessary to carry out hydrothermal aging and heavy metal ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/24C10G11/18
Inventor 任世宏马燕青廖翼涛曹兰花樊江涛孙艳波张晨曦高雄厚张海涛王辰晨孙雪芹曹庚振
Owner PETROCHINA CO LTD
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