A method for rapid determination of the contents of various components in the steam distillation extraction process of turmeric-gardenia based on ultraviolet spectroscopy
A technology of steam distillation and ultraviolet spectroscopy, which is applied in the field of analysis of the production process of traditional Chinese medicine, to achieve the effect of low equipment cost, no damage to samples, and low analysis cost
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Embodiment 1
[0037] A method for quickly measuring the content of various components in the steam distillation extraction process of turmeric-gardenia based on ultraviolet spectroscopy, the method comprises the following steps:
[0038] (1) Collection of samples
[0039]Grind and sieve turmeric and gardenia medicinal materials to 20-80 mesh respectively, take 30g of powder and mix evenly, add 1500mL of distilled water, soak for 12 hours, and extract by steam distillation. When the medicinal solution boils, start timing, take 5mL samples of the distillate at the outlet of the condenser at the 15th and 30th minutes respectively, and then sample 5mL every 30 minutes, and stop sampling when the total volume of the distillate (including the sampling volume) reaches 1000mL . According to the above conditions, 11 batches of extraction experiments were carried out, and the obtained samples were used as the training set.
[0040] After changing one of the above extraction conditions, five batches...
Embodiment 2
[0068] A method for quickly measuring the content of various components in the steam distillation extraction process of turmeric-gardenia based on ultraviolet spectroscopy, the method comprises the following steps:
[0069] (1) Collection of samples
[0070] (2) Determination of the content of each component in the sample set
[0071] (3) Sample ultraviolet spectrum collection
[0072] (4) Establishment of quantitative calibration model
[0073] (5) Application of quantitative calibration model
[0074] Completed step (1)~(4) in the development process of the inventive method, concrete process can refer to embodiment 1 step (1)~(4), therefore, in the application of the inventive method, can directly carry out step ( 5) As follows: the medicinal materials of turmeric and gardenia are crushed and sieved to 10-20 meshes respectively, 30g of powders are taken and mixed evenly, add 1500mL of distilled water, soak for 12 hours, extract by steam distillation, wait for the liquid t...
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