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A dd5 single crystal superalloy turbine blade corrosion method

A technology of superalloy and turbine blades, which is applied in the field of turbine blade production, can solve the problems of excessive corrosion of the surface structure and appearance size of castings, volatile hydrochloric acid, and reduced product qualification rate, so as to achieve clear display of surface grains and defects and repeated production The effect of good performance and controllable process parameters

Active Publication Date: 2019-10-15
ANHUI YINGLIU HANGYUAN POWER TECH CO LTD
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AI Technical Summary

Problems solved by technology

After the single crystal turbine blade is casted, it is necessary to use corrosion method to show the grain growth during melting and solidification. The traditional method uses hydrochloric acid hydrogen peroxide (9:1) method for corrosion. Hydrochloric acid is very volatile, and hydrogen peroxide and hydrochloric acid solution also produce chemical reactions, resulting in The composition of the solution is unstable, which can easily lead to unclear corrosion effect or local excessive corrosion, resulting in unqualified casting surface structure and appearance size, thereby reducing the product qualification rate

Method used

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Effect test

Embodiment 1

[0019] A DD5 single crystal superalloy turbine blade corrosion method, it comprises the following steps:

[0020] 1) Sand blasting: choose 8 mm sand blasting machine nozzle, adjust the compressed air power to 6 bar, 120-220 mesh sand, and form an angle of 45° with the surface of the casting to be sand blasted, and the distance between the sand blasting machine nozzle and the spray casting surface is 30-50 mm, the injection time is 5 minutes, and then remove the oxide layer and pollutants on the surface of the casting, and at the same time generate compressive stress on the surface of the casting, so that the surface of the casting is in an activated state;

[0021] 2) Primary chemical corrosion: using 40% ferric chloride solution and 37% hydrochloric acid solution to match the corrosion solution, the casting in step 1) is chemically etched, and the chemical corrosion time is 9 minutes;

[0022] 3) One-time cleaning: use an ultrasonic cleaning machine to clean the reactants adh...

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Abstract

The invention discloses a corroding method of a DD5 single-crystal high-temperature alloy turbine blade. The method includes the following steps of firstly, sand blasting; secondly, primary chemical corroding, wherein a 40% ferric trichloride solution and a 37% hydrochloric acid solution are used for preparing a corroding solution, and chemical erosion is conducted on a cast in the first step for9 minutes; thirdly, primary washing, reactants adhering to the surface of the cast and generated during chemical erosion in the second step are washed away through an ultrasonic washing machine, the ultrasonic frequency is 20 KHz, the water temperature is 50 DEG C, and the washing time is 5 minutes; fourthly, secondary electrochemical corroding; fifthly, secondary washing; sixthly, tertiary electrochemical corroding; seventhly, neutralizing, wherein the cast in the six step is placed in a 5% NaHCO3 room-temperature solution to be soaked for 3 minutes, and acid liquid on the surface of the castis neutralized; eighthly, drying. The corrosion effect is clear, and it can be avoided that due to local excessive corrosion, surface structure and appearance size of the cast are not qualified.

Description

technical field [0001] The invention relates to the technical field of turbine blade production, in particular to a DD5 single crystal superalloy turbine blade corrosion method. Background technique [0002] DD5 single crystal superalloy is the second generation cast single crystal master alloy developed in my country. Single crystal turbine blade means that the entire turbine blade is composed of one crystal grain. After the single crystal turbine blade is casted, it is necessary to use corrosion method to show the grain growth during melting and solidification. The traditional method uses hydrochloric acid hydrogen peroxide (9:1) method for corrosion. Hydrochloric acid is very volatile, and hydrogen peroxide and hydrochloric acid solution also produce chemical reactions, resulting in The composition of the solution is unstable, which can easily cause unclear corrosion effect or local excessive corrosion, resulting in unqualified casting surface structure and appearance siz...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23F1/28C25F3/02
Inventor 杜应流杨家博葛丙明程耀先蔡福宜
Owner ANHUI YINGLIU HANGYUAN POWER TECH CO LTD
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