Surfactant for drilling fluid and preparation method thereof

A surfactant and drilling fluid technology, applied in the field of petroleum drilling aids, can solve problems such as no guidance plan, complex production process, and land environmental pollution, and achieve reduction of downhole complex accidents, simplified process steps, and low cycle density Effect

Active Publication Date: 2018-12-21
石家庄华莱鼎盛科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Some of the above technologies use raw materials with strong alkalinity, large molecular weight, not easy to degrade, and easy to cause environmental pollution to the land
And the production process is complicated and the cost is high
The above technologies have a great impact on how to make the surfactant used in drilling fluid have strong compression resistance, ensure that the drilling fluid has a low circulation density under high pressure at the bottom of the well, enhance the ability to carry cuttings in suspension, reduce complex downhole accidents, and improve drilling efficiency. Quality and efficiency, while having environmental protection functions, did not give a specific guidance plan

Method used

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  • Surfactant for drilling fluid and preparation method thereof
  • Surfactant for drilling fluid and preparation method thereof
  • Surfactant for drilling fluid and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028]Embodiment 1: the tensio-active agent for drilling fluid of the present invention is made from the raw material of following weight ratio (weight parts, mass parts):

[0029]

[0030] Described mineral oil is the composition of No. 5 white oil, No. 7 white oil two kinds of raw materials, and the weight ratio of No. 5 white oil and No. 7 white oil is 1: 0.5; Described emulsifier is Tween T- 60. The composition of Tween T-80, the weight ratio of Tween T-60 to Tween T-80 is 1:2.

[0031] The preparation method of described surfactant for drilling fluid comprises following processing steps: 1. take by weighing raw material mineral oil (being No. 5 white oil, No. 7 white oil), oleic acid n-butanol, liquid paraffin, Methyl silicone oil, emulsifier (ie Tween T-60, Tween T-80), put each raw material into the reaction kettle, mix each raw material fully to obtain a mixture; ②Then emulsify the mixture, the emulsification temperature 60°C, the emulsification time is 2h, and the...

Embodiment 2

[0032] Embodiment 2: the tensio-active agent for drilling fluid of the present invention is made from the raw material of following weight ratio (weight parts, mass parts):

[0033]

[0034] Described mineral oil is No. 7 white oil; Described emulsifier is the composition of Tween T-80, emulsifier S-80, and the weight ratio of Tween T-80 and emulsifier S-80 is 1: 0.5.

[0035] The preparation method of described surfactant for drilling fluid comprises following processing steps: 1. take by weighing raw material mineral oil, oleic acid n-butyl alcohol, liquid paraffin, methyl silicone oil, emulsifying agent (being Tween T- 80. Emulsifier S-80), put each raw material into the reaction kettle, fully mix each raw material to obtain a mixture; ②Then emulsify the mixture, the emulsification temperature is 70 ° C, the emulsification time is 1.5h, the emulsification process After the process is completed, the intermediate product is obtained; ③ cool down the intermediate product o...

Embodiment 3

[0036] Embodiment 3: the tensio-active agent for drilling fluid of the present invention is made from the raw material of following weight ratio (weight parts, mass parts):

[0037]

[0038] Described mineral oil is No. 5 white oil; Described emulsifier is emulsifier S-80.

[0039] The preparation method of the described surfactant for drilling fluid comprises the following process steps: 1. Weigh the raw materials mineral oil, oleic acid n-butanol, liquid paraffin, methyl silicone oil and emulsifier according to the above weight ratio, and add each raw material to the reaction In the kettle, the raw materials are fully mixed to obtain the mixture; ②Then the mixture is emulsified, the emulsification temperature is 80 ° C, the emulsification time is 1h, and the intermediate product is obtained after the emulsification process is completed; ③ The intermediate product obtained in step ② Cool down, add 1 part of ethyl p-hydroxybenzoate at 50°C, make it fully mixed, and discharg...

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Abstract

The invention provides a surfactant for drilling fluid and a preparation method of the surfactant. The surfactant is prepared from raw materials as follows: mineral oil, n-butyl alcohol oleate, liquidparaffin, methyl silicone oil, an emulsifier and ethyl p-hydroxybenzoate, wherein the mineral oil is one or two of No.5 white oil and No.7 white oil. The preparation method comprises steps as follows: the mineral oil, n-butyl alcohol oleate, liquid paraffin, methyl silicone oil and the emulsifier are added to a reactor and are sufficiently mixed and stirred; the materials in the reactor are heated and emulsified; ethyl p-hydroxybenzoate is added at certain temperature, the materials are sufficiently mixed and stirred, and the surfactant is obtained after cooling. The surfactant is good in performance and prepared with a simple process, has higher resistance to compression and guarantees that the drilling fluid has lower circulating density and higher suspended rock debris carrying capacity at the shaft bottom under high pressure, complex underground accidents are avoided or reduced effectively, and drilling quality and efficiency are improved; the surfactant still has good performanceat high temperature, can be resistant to 10% compound brine pollution and has good inhibiting performance for lubrication.

Description

technical field [0001] The invention relates to a petroleum drilling aid, in particular to a surfactant for drilling fluid. The invention also relates to a preparation method of the surfactant for drilling fluid. Background technique [0002] Drilling fluid is an important fluid in drilling engineering, and its performance is directly related to the quality of drilling, and plays a crucial role in the oil recovery efficiency of an oil field. There are many kinds of surfactants on the market at present, but they often cannot be both efficient and environmentally friendly. Currently commonly used surfactants that can meet environmental protection requirements have certain deficiencies in their performance. It is difficult to effectively surface active and ensure the high-efficiency performance of drilling fluids. [0003] The inventor retrieved the following relevant patent documents: CN104962247A discloses a lubricating and plugging agent for drilling fluid and its preparat...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/035C09K8/04
CPCC09K8/035C09K8/04
Inventor 陈利赵秀平
Owner 石家庄华莱鼎盛科技有限公司
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