Chinese herbal medicine mouthwash and preparation method thereof
A technology for mouthwash and Chinese herbal medicine, applied in the field of Chinese herbal medicine mouthwash and its preparation, can solve the problems of easy coloring of the surface of teeth and oral mucosa, poor halitosis removal effect, reduction of oral bacteria and the like, and achieve prevention of dental calculus and prevention of dental The effect of aging and improving breath
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Embodiment 1
[0034] Preparation of cinnamon extract: crush cinnamon to 40 mesh, add water to soak for 2 hours, the amount of water added is 6 times the weight of cinnamon, add 0.5 times the weight of cinnamon NaCl, steam distillation for 5 hours; 3 The aqueous solution and the distilled product were fully shaken for 1 h, filtered, and dissolved in NaOH with 1 times the weight of cinnamon in the precipitate, extracted with ether with 3 times the weight of cinnamon, and saturated NaHSO 3 Purify the distillation product, filter it, add NaOH to the precipitate to dissolve it, extract it with ether, and remove the ether under reduced pressure to obtain cinnamon extract.
[0035] Preparation of mulberry leaf extract: Shred mulberry leaves and add water to decoct twice, add 10 times the weight of water to boil for the first time, and decoct for 1 hour to obtain decoction A and mulberry leaf residue; Boil the remaining mulberry leaf dregs for decoction, add 8 times the weight of water to boil, and...
Embodiment 2
[0042] Preparation of cinnamon extract: crush cinnamon to 45 mesh, soak in water for 2.5 hours, the amount of water added is 6 times the weight of cinnamon, add 0.5 times the weight of cinnamon NaCl, steam distillation for 5.5 hours; use the same amount of distilled product saturated NaHSO 3 The aqueous solution and the distilled product were fully shaken for 1 hour, filtered, and NaOH 1 times the weight of cinnamon was added to the precipitate to dissolve it, extracted with ether 3 times the weight of cinnamon, and the ether was removed under reduced pressure to obtain a cinnamon extract.
[0043] Preparation of mulberry leaf extract: Shred mulberry leaves and add water to decoct twice, add 12 times the weight of water to boil for the first time, and decoct for 1 hour to obtain decoction A and mulberry leaf residue; Boil the remaining mulberry leaf dregs for decoction, add 9 times the weight of water to boil, and decoct for 1.5 hours to obtain decoction B; combine the two dec...
Embodiment 3
[0050] Preparation of cinnamon extract: crush cinnamon to 50 mesh, add water to soak for 3 hours, the amount of water added is 6 times the weight of cinnamon, add 0.5 times the weight of cinnamon NaCl, steam distillation for 6 hours; 3 The aqueous solution and the distilled product were fully shaken for 1 hour, filtered, and NaOH 1 times the weight of cinnamon was added to the precipitate to dissolve it, extracted with ether 3 times the weight of cinnamon, and the ether was removed under reduced pressure to obtain a cinnamon extract.
[0051] Preparation of mulberry leaf extract: Shred mulberry leaves and add water to decoct twice, add 13 times the weight of water to boil for the first time, and decoct for 1.5h to obtain decoction A and mulberry leaf residue; Decoct the remaining mulberry leaf dregs for decoction, add 10 times the weight of water to boil, and decoct for 1.5 hours to obtain decoction B; combine the two decoctions and filter through a 350-mesh sieve to obtain the...
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