Floppers herb flavone compound LEF

A technology of rooting and rooting on the ground, which is applied to the preparation of sugar derivatives, sugar derivatives, and sugar derivatives, and can solve problems such as retention

Inactive Publication Date: 2007-03-07
EAST CHINA UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] From international and domestic research reports, it can be seen that the root of the root shows good medicinal effects from the traditional and modern perspectives, but the separation and preparation of the flavonoids of the root of the root are still only at the laboratory scale.

Method used

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  • Floppers herb flavone compound LEF
  • Floppers herb flavone compound LEF
  • Floppers herb flavone compound LEF

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0035] 1. Resin pretreatment

[0036] (1) Macroporous Adsorption Resin Put the resin into the column, rinse with acetone 2 to 3 times (volume ratio of liquid to solid) first, then wash with deionized water 3 to 4 times (volume ratio of liquid to solid), and then continue to use Wash with 1mol / L hydrochloric acid aqueous solution with the same volume as the resin, and let it stand for 8 to 12 hours after completion, wash the column with deionized water to neutrality, continue to wash the column with 1mol / L NaOH solution until the effluent is strongly alkaline, after completion After standing still for 3-12 hours, wash the column with deionized water until neutral.

[0037] (2) Polyamide Take polyamide powder and soak it in 90-95% ethanol aqueous solution with a volume of 1-2 times (solid-liquid volume ratio), stir constantly, remove air bubbles, and put it into a chromatography column. Wash with 3-4 times (solid-to-liquid volume ratio) volume of 90-95% ethanol aqueous solution...

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Abstract

Air plant flavone compound LEF is carried out by taking leaves of air plant flavone as main materials, breaking, extracting, filtering, macro-porous resin adsorbing, stripping, extracting polyamide chromatographing, obtaining end products with purity 51.23%, preparing object compound pure products by HPLC, obtaining spectrogram by ultraviolet, mass spectrum and nuclear magnetic resonance experimenting, analyzing spectrogram, and obtaining the compound quercetin-(3-1)- alpha -L-rhamnose-(2-1)- beta-D-xylose with molecular formula C26H28O15.

Description

technical field [0001] The invention relates to Luodishenggen Extract Flavonoids, a flavonoid compound LEF (Luodishenggen Extract Flavonoids) isolated and prepared from the leaves of the herbaceous plant. Background technique [0002] Bryophyllum pinnatum LF OKEN (Bryophyllum pinnatum LF OKEN) is a perennial succulent herb whose leaves can be harvested throughout the year. Domestically, it is widely distributed in Guangdong, Guangxi, Fujian, Taiwan and Yunnan. [0003] In the world, there have been some researches on the traditional and modern medical value of the roots and roots. It is reported that Nigeria and other countries have carried out preliminary medical value evaluation on the roots and leaves of the roots and leaves. The traditional medical value of roots and leaves is basically reflected in the following aspects: (1) treatment of brain diseases, stroke and high blood pressure (2) preparation of antibacterial and anti-inflammatory agents, etc. (3) treatment of c...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07H17/07C07H1/08
Inventor 徐殿胜曹宏夏杰陈国豪陆兵
Owner EAST CHINA UNIV OF SCI & TECH
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