2-propyl enanthaldehyde preparation method
A kind of technology of propyl heptanal and propyl group, applied in the field of preparing compound 2-propyl heptanal, can solve the problems such as the preparation method of 2-propyl heptanal has not been found yet
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[0014] The selective hydrogenation of 2-propyl-2-heptenal was carried out in a two-stage serial fixed-bed flow system with reflux as shown in the accompanying drawing. Before the reaction starts, the catalyst needs to be pre-reduced. At 200°C and under the reaction pressure, the catalyst is reduced with hydrogen flow for 12 hours, and then lowered to the reaction temperature. The selective hydrogenation reaction is carried out at a certain temperature and pressure, and the alkenal raw material is pumped from the upper end of the reactor at a certain flow rate, and the tail gas flow rate is controlled to determine the molar ratio of the hydrogen to the alkenal. After the system was stabilized, samples were collected and analyzed regularly.
[0015] Table 1 is the reaction conditions tested, LOOP1 is the first-stage reactor loop, and LOOP2 is the second-stage reactor loop. Wherein the space velocity is measured by the liquid hourly volumetric space velocity of fresh raw materia...
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