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33results about How to "Reduce the draining speed" patented technology

Self gas generation foam-gel profile control agent prepared from oilfield reinjection water as well as preparation method and application thereof

ActiveCN103834376AControl generation timeAdjust crosslinking timeDrilling compositionCross-linkSalt resistance
The invention relates to a self gas generation foam-gel profile control agent prepared from oilfield reinjection water and a preparation method and an application of the agent. The self gas generation foam-gel profile control agent is prepared from the following components: 0.1-0.3% of polyacrylamide, 0.1-0.3% of a cross-linking agent, 2.0% of NH4Cl, 1.6% of NaNO2, 0.05-0.15% of a catalyst, 0.2-0.5% of a foaming agent, 1-5% of a stabilizing agent and the balance of oilfield reinjection water. The preparation method comprises the steps of dissolving polyacrylamide by using oilfield reinjection water firstly, and secondly adding other components to be uniformly dissolved. The self gas generation foam-gel profile control agent is used for profile control on oilfield reinjection water, and can be also applied to increase production through fracturing, acidification and fuel scavenge; the foam-gel profile control agent is good in salt resistance, the liquid can be prepared by using oilfield reinjection water with high-salinity temperature, the water resource is saved, and the oil-water pollution is reduced; the agent is not cross-linked with being placed at high temperature for a long time, so that construction security is ensured; after the agent is filled into a stratum, foam and gel cross-linking is formed simultaneously, and the foams are uniformly dispersed in the gel with high strength.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Filtering basket type ultrasonic extraction device for biological effective components

The invention provides a filtering basket type ultrasonic extraction device for biological effective components, which relates to an extraction device for biological effective components. The invention solves the problems that incomplete filtration of an extract and slow discharge speed of the extract exist in the traditional intermittent type ultrasonic extraction device and a solid material blocks a liquid outlet. In the invention, a filtering basket is connected with an electric lifter by a suspension rope and installed in a liquid storage tank, an annular gas spray head is installed in the filtering basket, at least two ultrasonic vibration boxes are annularly arrayed on the outer wall of the filtering basket, a gas passing pipe is installed on the inner wall of the filtering basket, a liquid discharge pipe is installed on the lower end face of the liquid storage tank, and at least two of the ultrasonic vibration boxes are respectively connected with a control box outside the liquid storage tank by a wire cable. The invention realizes that the extract does not need to be filtered again, and avoids that slag is deposited at the bottom of the liquid storage tank so as to slow up liquid discharge speed and even block the liquid outlet; by the split design of the liquid storage tank and the filtering basket, the invention discharges liquid quickly and is convenient to disassemble and wash the extraction device.
Owner:HARBIN INST OF TECH

Medium-high-temperature strong plugging hard rubber micro-foam drilling fluid and preparation method thereof

The invention discloses a medium-high temperature strong plugging hard rubber recyclable foam drilling fluid and a preparation method thereof. A low-molecular-weight high-temperature-resistant foam stabilizer, a wetting agent and a bubble film density lightening agent are added into clear water to form a temperature-resistant hard rubber base solution. Sodium bentonite, an alkaline regulator, a sulfonate polymer filtrate reducer, a foaming agent, a temperature-resistant resin filtrate reducer and a foam surface viscosity regulator are added into the temperature-resistant hard rubber base solution to form the medium-high temperature hard rubber recyclable micro-foam drilling fluid or completion fluid. A low-density blocking agent is added and stirred to form the medium-high temperature strong plugging hard rubber micro-foam drilling fluid or completion fluid. The medium-high-temperature strong plugging recyclable foam fluid is low in solid phase content, strong in membrane structure and excellent in foam stabilizing effect before and after medium-high temperature; and the recyclable times and the plugging effect of the completion fluid after the micro-foam drilling fluid can be improved, the loss of the drilling fluid is reduced, the safe and high-effect recyclable micro-foam drilling and completion fluid can be used for exploiting medium-high-temperature and low-pressure easily-leaking oil and gas resources, geothermal wells and the like, and the deep well drilling requirement is met.
Owner:中石化石油工程技术服务有限公司 +2

Self-generating foam jelly profile control agent prepared with oilfield reinjection water and its preparation method and application

ActiveCN103834376BControl generation timeAdjust crosslinking timeDrilling compositionSalt resistanceCross-link
The invention relates to a self gas generation foam-gel profile control agent prepared from oilfield reinjection water and a preparation method and an application of the agent. The self gas generation foam-gel profile control agent is prepared from the following components: 0.1-0.3% of polyacrylamide, 0.1-0.3% of a cross-linking agent, 2.0% of NH4Cl, 1.6% of NaNO2, 0.05-0.15% of a catalyst, 0.2-0.5% of a foaming agent, 1-5% of a stabilizing agent and the balance of oilfield reinjection water. The preparation method comprises the steps of dissolving polyacrylamide by using oilfield reinjection water firstly, and secondly adding other components to be uniformly dissolved. The self gas generation foam-gel profile control agent is used for profile control on oilfield reinjection water, and can be also applied to increase production through fracturing, acidification and fuel scavenge; the foam-gel profile control agent is good in salt resistance, the liquid can be prepared by using oilfield reinjection water with high-salinity temperature, the water resource is saved, and the oil-water pollution is reduced; the agent is not cross-linked with being placed at high temperature for a long time, so that construction security is ensured; after the agent is filled into a stratum, foam and gel cross-linking is formed simultaneously, and the foams are uniformly dispersed in the gel with high strength.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Preparation method for temperature-resistant salt-tolerant oil-displacing foaming agent

The invention relates to the technical field of preparation of foaming agents used for oil recovery in an oil reservoir, and in particular relates to a preparation method for a temperature-resistant salt-tolerant oil-displacing foaming agent. According to the method provided by the invention, firstly a reaction is performed to obtain a linear alkyl benzene sulfonate, the linear alkyl benzene sulfonate is compounded with alkyl diphenyl ether sodium disulfonate and polyacrylamide to obtain a novel substance, so that thermal stability is enhanced, and the temperature resistance and salt toleranceof the oil-displacing foaming agent are improved; a hydrogen bond is easily formed in polyacrylamide, so that the mineralization resistance and salt tolerance of the substance are improved; a titanate coupling agent is used to modify quartz sand powder, and the modified quartz sand powder, yeast powder and white sugar are subjected to fermentation together, so that the temperature resistance of the alkyl benzene sulfonate is enhanced at the high temperature, and the temperature resistance of the oil-displacing foaming agent is improved; and a polyether, a sodium carbonate solution and a sulfonated castor oil foam stabilizer are added, so that the salt tolerance of the foaming agent can be enhanced, the stability of foam is improved, the temperature resistance and salt tolerance of the oil-displacing foaming agent are further improved, and the oil-displacing foaming agent has broad application prospects.
Owner:王敏

Filtering basket type ultrasonic extraction device for biological effective components

The invention provides a filtering basket type ultrasonic extraction device for biological effective components, which relates to an extraction device for biological effective components. The invention solves the problems that incomplete filtration of an extract and slow discharge speed of the extract exist in the traditional intermittent type ultrasonic extraction device and a solid material blocks a liquid outlet. In the invention, a filtering basket is connected with an electric lifter by a suspension rope and installed in a liquid storage tank, an annular gas spray head is installed in the filtering basket, at least two ultrasonic vibration boxes are annularly arrayed on the outer wall of the filtering basket, a gas passing pipe is installed on the inner wall of the filtering basket, a liquid discharge pipe is installed on the lower end face of the liquid storage tank, and at least two of the ultrasonic vibration boxes are respectively connected with a control box outside the liquid storage tank by a wire cable. The invention realizes that the extract does not need to be filtered again, and avoids that slag is deposited at the bottom of the liquid storage tank so as to slow upliquid discharge speed and even block the liquid outlet; by the split design of the liquid storage tank and the filtering basket, the invention discharges liquid quickly and is convenient to disassemble and wash the extraction device.
Owner:HARBIN INST OF TECH

A kind of high temperature hard rubber recyclable foam drilling fluid and preparation method thereof

The invention discloses a high-temperature hard rubber recyclable foam drilling fluid and a preparation method thereof. 0.2~0.8 parts of low molecular weight anti-high temperature foam stabilizer, 1~2 parts of bubble film density reducing agent and 0.1~0.2 parts of high temperature wetting agent are pre-prepared into high temperature resistant hard rubber base liquid in clear water, and then the temperature resistant sodium bentonite is mixed. 0~3 parts of alkaline regulator, 0.3~0.5 parts of high temperature foaming agent, 0.1~0.5 parts of high temperature and salt resistant fluid loss reducer and 1~3 parts of high temperature resin fluid loss reducer and mixed evenly. Add it into the high temperature resistant base liquid while stirring, and stir it with a low-speed strong stirrer for 5 to 7 hours. The invention has low solid phase content, strong membrane structure, excellent foam stabilization effect under high temperature environment, improves the recirculation times of the completion fluid after the micro-foam drilling fluid and the loss-stopping effect under high temperature and high pressure, and makes the recirculatable micro-foam drilling and completion fluid safe. It is efficiently used in the exploitation of medium, high temperature and low pressure oil and gas resources, geothermal wells or salt gypsum layers, etc., to meet the drilling needs of deep and ultra-deep wells.
Owner:中石化石油工程技术服务有限公司 +2

A kind of concrete air-entraining agent and preparation method thereof

The invention discloses a concrete air entraining agent and a preparation method thereof and belongs to the field of concrete additives. According to the concrete air entraining agent, erucylamide, hydrochloric acid and the like are used as raw materials to synthesize a long-carbon-chain cationic surfactant to reduce the surface tension; then isopropanol is used as a solvent to react, and gas generated in a hydration process can be uniformly squeezed and entrained, so that the compactness is improved; polyaspartic acid is modified through fumaric acid and carboxylic acid and amide groups are introduced so that the air entraining efficiency is improved; and polyethylene vinyl acetate and polyvinyl versatate are added and can form a film when meeting water, so that the bending strength and permeability resistance of mortar are improved and the whole performance in an concrete air entraining process is improved. According to the concrete air entraining agent, foam is formed through the surfactant to close pores, so that the compactness and the water resisting performance are improved. By adopting the concrete air entraining agent, the problems of a current concrete air entraining agent that the foam stability is poor and the influence on the hardening strength of concrete is great are solved.
Owner:四川宏业商品混凝土有限公司

A kind of medium-high temperature hard rubber recyclable foam drilling fluid and preparation method thereof

The invention discloses a medium-high temperature hard rubber recyclable foam drilling fluid and a preparation method thereof. Add low molecular weight anti-high temperature foam stabilizer to clear water. After dispersing and dissolving, add wetting agent and foam film density reducing agent successively. Stir well and let stand to ensure full swelling to form a temperature resistant hard base liquid. Accurately weigh the sodium bentonite, alkaline regulator, sulfonate polymer fluid loss reducer, foaming agent, temperature-resistant resin fluid loss reducer and foam surface viscosity regulator, mix them evenly, and add the temperature-resistant hard gum base while stirring. medium and high temperature hard rubber can be circulated in micro-foam drilling fluid or completion fluid. The medium and high temperature recyclable foam fluid of the invention has low solid phase content, strong membrane structure and excellent foam stabilization effect, and can resist saturated NaCl and 25% CaCl 2 , to increase the recirculation times of the completion fluid after the micro-foam drilling fluid, so that the recyclable micro-foam drilling and completion fluid can be safely and efficiently used in the exploitation of medium, high temperature and low pressure leaky oil and gas resources and geothermal wells.
Owner:中石化石油工程技术服务有限公司 +2

High-temperature ebonite recyclable foam drilling fluid and preparation method thereof

The invention discloses a high-temperature ebonite recyclable foam drilling fluid and a preparation method thereof. The preparation method comprises the following steps: pre-preparing a high-temperature-resistant ebonite base solution from 0.2-0.8 part of a low-molecular-weight high-temperature-resistant foam stabilizer, 1-2 parts of a bubble film density lightening agent and 0.1-0.2 part of a high-temperature wetting agent in clear water; and uniformly mixing 0-3 parts of temperature-resistant sodium bentonite, 0-0.1 part of an alkaline regulator, 0.3-0.5 part of a high-temperature foaming agent, 0.1-0.5 part of a high-temperature-resistant salt-resistant filtrate reducer and 1-3 parts of a high-temperature-resistant resin filtrate reducer, adding the mixture into the high-temperature-resistant base solution while stirring, and conducting stirring for 5-7 hours by using a low-speed strong stirrer. The solid phase content is low, and the membrane structure is strong; and the foam stabilizing effect is excellent in a high-temperature environment, the cycle index of the completion fluid after the micro-foam drilling fluid is increased, the leaking stoppage effect under high temperature and high pressure is improved, the safe and high effect of the recyclable micro-foam drilling and completion fluid is used for exploiting medium-high-temperature low-pressure easily-leaking oil and gas resources, geothermal wells or salt-gypsum layers and the like, and the drilling requirements of deep wells and ultra-deep wells are met.
Owner:中石化石油工程技术服务有限公司 +2

A kind of medium-high temperature strong plugging hard rubber micro-foam drilling fluid and preparation method thereof

The invention discloses a medium-high temperature strong plugging hard rubber recyclable foam drilling fluid and a preparation method thereof. Add low molecular weight anti-high temperature foam stabilizer, wetting agent and foam film density reducing agent to water to form temperature resistant hard base liquid. Add sodium bentonite, alkaline regulator, sulfonate polymer fluid loss reducer, foaming agent, temperature resistant resin fluid loss reducer and foam surface viscosity modifier into the temperature resistant hard gum base liquid to form medium and high temperature hard gum Circulating microfoam drilling fluid or completion fluid. Add low-density plugging agent and stir to form medium and high temperature strong plugging hard rubber micro-foam drilling fluid or completion fluid. The medium and high temperature strong plugging recyclable foam fluid of the invention has low solid phase content, strong membrane structure, and excellent foam stabilization effect before and after medium and high temperature; it can improve the circulation times of the completion fluid after the micro-foam drilling fluid and the effect of plugging, and reduce the loss of drilling fluid , so that the recyclable micro-foam drilling and completion fluid can be safely and efficiently applied to the exploitation of medium, high temperature and low pressure oil and gas resources, geothermal wells, etc., which are easy to leak, and meet the needs of deep well drilling.
Owner:中石化石油工程技术服务有限公司 +2
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