Method for preparing aspartic acid
A technology of potassium aspartate and aspartic acid, which is applied in the chemical field, can solve the problems of preparation product safety hazards, high related substances, and low efficiency, so as to improve production efficiency and product quality, increase product yield, and reduce The effect of production costs
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Embodiment 1
[0028] Add 1340 milliliters of purified water in the flask, add 56.1 grams of potassium hydroxide under stirring, after all dissolve, add 133.1 grams of L-aspartic acid. After the addition, reflux for 2 hours, and adjust the pH of the solution to 6.0-8.0 with potassium hydroxide and aspartic acid. After filtration, about 80% of the solvent (water) was evaporated from the filtrate under reduced pressure, and the obtained viscous substance was added into 1340 ml of ethanol at -40° C. under stirring, and a large amount of solids were formed while stirring. After adding, let stand for 1 hour. Centrifuge and dry under reduced pressure at 50°C to obtain 181.3 g of potassium L-aspartate, with a yield of 96.3%. The structure of the potassium L-aspartate prepared in this example was confirmed and consistent with that reported in the literature.
Embodiment 2
[0030] Add 1400 milliliters of purified water in the flask, add 69.1 grams of potassium carbonate under stirring, then slowly add 133.1 grams of L-aspartic acid. After the addition, reflux for 2 hours, and adjust the pH of the solution to 6.0-8.0 with potassium hydroxide and aspartic acid. After filtration, about 70% of the solvent (water) was evaporated from the filtrate under reduced pressure, and the obtained viscous substance was added into 1400 ml of ethanol at -80° C. under stirring, and a large amount of solids were formed while stirring. After adding, let stand for 1 hour. Centrifuge and dry under reduced pressure at 50°C to obtain 179.0 g of potassium L-aspartate, with a yield of 95.1%. The structure of the potassium L-aspartate prepared in this example was confirmed and consistent with that reported in the literature.
Embodiment 3
[0032]Add 1200 milliliters of purified water in the flask, add 100.1 grams of potassium bicarbonate under stirring, then slowly add 133.1 grams of L-aspartic acid. After the addition, reflux for 2 hours, and adjust the pH of the solution to 6.0-8.0 with potassium hydroxide and aspartic acid. After filtration, about 85% of the solvent (water) was evaporated from the filtrate under reduced pressure, and the obtained viscous substance was added into 1200 ml of -60°C ethanol with stirring, and a large amount of solids were formed while stirring. After adding, let stand for 1 hour. Centrifuge and dry under reduced pressure at 50°C to obtain 183.1 g of potassium L-aspartate with a yield of 97.3%. The structure of the potassium L-aspartate prepared in this example was confirmed and consistent with that reported in the literature.
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