Oolong tea extract extracted from mineral ether and preparation and use thereof
A technology of petroleum ether extraction and oolong tea, which is applied to the application and preparation of tobacco, essential oils/spices, etc., to achieve the effect of improving the taste aftertaste, easy operation and simple process
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Embodiment 1
[0029] Weigh 500 grams of oolong tea with an electronic balance, put it into a flask, add 2500ml of medical grade petroleum ether with a boiling point of 30-60°C, soak for 10 hours at 20°C, separate the solid and liquid with a Bush funnel, collect the clear liquid, and obtain The liquid was distilled and concentrated for 2.0 h at a vacuum of 0.05 MPa and a distillation temperature of 28° C., and the solvent was removed to obtain 1.2 g of extract.
Embodiment 2
[0031] Weigh 1,000 grams of oolong tea with an electronic balance, put it into a Erlenmeyer flask, add 10,000ml of petroleum ether with a boiling point of 60-90°C, soak it at 30°C for 20 hours, use a Bush funnel for solid-liquid separation, and collect the clear liquid. Distill and concentrate for 1.0 h at a vacuum of 0.1 MPa and a distillation temperature of 30° C., and remove the solvent to obtain 6.75 g of extract.
Embodiment 3
[0033] Weigh 1,000 grams of oolong tea with an electronic balance, put it into a Erlenmeyer flask, add 15,000ml of petroleum ether with a boiling point of 30-60°C, soak it at 15°C for 10 hours, use a Bush funnel to separate the solid from the liquid, and collect the clear liquid. The vacuum degree is 0.01MPa, the distillation temperature is 25°C and the distillation is concentrated for 1.5h, and the solvent is removed to obtain 6.8g of extract.
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